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Rocking-curve Measurements (rocking-curve + measurement)
Selected AbstractsRapid determination of stress factors and absolute residual stresses in thin filmsJOURNAL OF APPLIED CRYSTALLOGRAPHY, Issue 6 2006E. Eiper A methodology is presented that allows the determination of experimental stress factors in thin films on the basis of static diffraction measurements. The approach relies on the characterization of thin films deposited on a monocrystalline substrate serving as a mechanical sensor. Rocking-curve measurements of the symmetrical reflections of the substrate are used to determine the substrate curvature and subsequently the macroscopic stress imposed on the film. The elastic strain in the film is determined by lattice-spacing measurement at different sample tilt angles. The calculated experimental stress factors are applied to thin films deposited on other types of substrates and are used to determine the absolute magnitude of the residual stress. The approach is applied to nanocrystalline TiN and CrN thin films deposited on Si(100) and steel substrates, characterized using a laboratory-type ,/, goniometer. [source] A lamellar model for the X-ray rocking curves of sagittally bent Laue crystalsACTA CRYSTALLOGRAPHICA SECTION A, Issue 1 2003Z. Zhong The use of sagittally bent asymmetric Laue crystals in horizontally focusing monochromators for high-energy synchrotron X-rays necessitates simulation of the X-ray reflectivity by such crystals. Based on the theory of the lattice distortion in the diffraction plane of sagittally bent Laue crystals, a lamellar model was developed to predict their rocking curves. The model was experimentally verified by rocking-curve measurements from various reflections on silicon crystals of four representative orientations, sagittally bent to various radii, using X-rays of 67,keV energy. [source] Accurate rocking-curve measurements on protein crystals grown in a homogeneous magnetic field of 2.4,TACTA CRYSTALLOGRAPHICA SECTION D, Issue 6 2004Daniel Lübbert Differences in mosaicity between lysozyme crystals grown inside and outside a homogeneous magnetic field of 2.4,T and with and without agarose gel were investigated by X-ray diffraction rocking-curve measurements. High angular resolution was achieved using an Si(113) four-reflection Bartels monochromator. The results show that (i) all crystals were highly perfect, (ii) the mosaicities were clearly anisotropic and (iii) the mosaicities varied more strongly within each group of crystals (grown under identical conditions) than the average values across groups. In particular, the effect of the magnetic field on crystal mosaicity was found to be very small. Finally, the spatial distribution of mosaic blocks inside a protein crystal was visualized with a novel diffraction technique using a high spatial resolution two-dimensional CCD detector. [source] | ||||||||||