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Green Protocol (green + protocol)
Selected AbstractsChemInform Abstract: A Green Protocol for Synthesis of Benzo-Fused N,S-, N,O- and N,N-Heterocycles in Water.CHEMINFORM, Issue 2 2009Qing-Yi Zhang Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a "Full Text" option. The original article is trackable via the "References" option. [source] Green Protocol for Annulation of the s-Triazine Ring on Thiazoles Using a Three-Component Coupling Strategy.CHEMINFORM, Issue 39 2006Lal Dhar S. Yadav Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract, please click on HTML or PDF. [source] An Efficient and Green Protocol for the Preparation of Cycloalkanols: A Practical Synthesis of Venlafaxine.CHEMINFORM, Issue 3 2005Subhash P. Chavan Abstract For Abstract see ChemInform Abstract in Full Text. [source] Efficient Solvent-Free Robinson Annulation Protocols for the Highly Enantioselective Synthesis of the Wieland,Miescher Ketone and AnaloguesADVANCED SYNTHESIS & CATALYSIS (PREVIOUSLY: JOURNAL FUER PRAKTISCHE CHEMIE), Issue 14-15 2009Ben Bradshaw Abstract A highly efficient (93% overall yield) and enantioselective (94% ee) synthesis of the Wieland,Miescher ketone (10-g scale) through a solvent-free Robinson annulation procedure is reported. The process involves only 1,mol% triethylamine as the base in the initial Michael process and the organocatalyst N -tosyl-(Sa)-binam- L -prolinamide (2,mol%) and benzoic acid (0.5,mol%) for the intramolecular aldol process. This green protocol is applied to a wide range of valuable building block analogues of the Wieland,Miescher ketone (10 examples). Among these, a noteworthy compound for terpene synthesis is the 8a-allyl derivative, which is prepared in 93% yield and 97% ee in a process allowing the recovery and reutilization of the organocatalyst. Furthermore, a one-pot, two-step process has also been developed. [source] |