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Factor Range (factor + range)

Distribution by Scientific Domains

Polymers and Materials Science	80%

Selected Abstracts

The evolution of the stress,strain fields near a fatigue crack tip and plasticity-induced crack closure revisited

FATIGUE & FRACTURE OF ENGINEERING MATERIALS AND STRUCTURES, Issue 1 2004
L. G. ZHAO
ABSTRACT The evolution of the stress,strain fields near a stationary crack tip under cyclic loading at selected R -ratios has been studied in a detailed elastic,plastic finite element analysis. The material behaviour was described by a full constitutive model of cyclic plasticity with both kinematic and isotropic hardening variables. Whilst the stress/strain range remains mostly constant during the cyclic loading and scales with the external load range, progressive accumulation of tensile strain occurs, particularly at high R -ratios. These results may be of significance for the characterization of crack growth, particularly near the fatigue threshold. Elastic,plastic finite element simulations of advancing fatigue cracks were carried out under plane-stress, plane-strain and generalized plane-strain conditions in a compact tension specimen. Physical contact of the crack flanks was observed in plane stress but not in the plane-strain and generalized plane-strain conditions. The lack of crack closure in plane strain was found to be independent of the material studied. Significant crack closure was observed under plane-stress conditions, where a displacement method was used to obtain the actual stress intensity variation during a loading cycle in the presence of crack closure. The results reveal no direct correlation between the attenuation in the stress intensity factor range estimated by the conventional compliance method and that determined by the displacement method. This finding seems to cast some doubts on the validity of the current practice in crack-closure measurement, and indeed on the role of plasticity-induced crack closure in the reduction of the applied stress intensity factor range. [source]

Small crack growth in combined bending,torsion fatigue of A533B steel

FATIGUE & FRACTURE OF ENGINEERING MATERIALS AND STRUCTURES, Issue 3 2001
J. Park
Crack growth rate data from bending, torsional and in-plane and 90° out-of-phase combined bending,torsional fatigue tests of A533B steel are presented. Crack growth was monitored from initial sizes generally in the range of 50,300 ,m to final sizes of several millimetres. Crack growth rate was found to vary linearly with crack size. Two approaches for correlating the A533B crack growth rate were evaluated, an effective strain-based intensity factor range and a method based on total cyclic strain energy density. The approaches were also evaluated using small crack growth data from the literature for SAE 1045 steel and Inconel 718 specimens tested under axial,torsional loadings. Predicted crack growth lives using both approaches were found to agree within a factor of two of observed lives for nearly all of the data examined. [source]

On the mechanism of fatigue failure in the superlong life regime (N>107 cycles).

FATIGUE & FRACTURE OF ENGINEERING MATERIALS AND STRUCTURES, Issue 11 2000
Part II: influence of hydrogen trapped by inclusions
High cycle fatigue fracture surfaces of specimens in which failure was initiated at a subsurface inclusion were investigated by atomic force microscopy and by scanning electron microscopy. The surface roughness Ra increased with radial distance from the fracture origin (inclusion) under constant amplitude tension,compression fatigue, and the approximate relationship: Ra,,,C,K,2I holds. At the border of a fish-eye there is a stretched zone. Dimple patterns and intergranular fracture morphologies are present outside the border of the fish-eye. The height of the stretch zone is approximately a constant value around the periphery of the fish-eye. If we assume that a fatigue crack grows cycle-by-cycle from the edge of the optically dark area (ODA) outside the inclusion at the fracture origin to the border of the fish-eye, we can correlate the crack growth rate da/dN, stress intensity factor range ,KI and Ra for SCM435 steel by the equation and by da/dN proportional to the parameter Ra,. Integrating the crack growth rate equation, the crack propagation period Np2 consumed from the edge of the ODA to the border of the fish-eye can be estimated for the specimens which failed at Nf,>,107. Values of Np2 were estimated to be ,1.0,×,106 for the specimens which failed at Nf,,,5,×,108. It follows that the fatigue life in the regime of Nf >107 is mostly spent in crack initiation and discrete crack growth inside the ODA. [source]

Creating Anti-Reflective Nanostructures on Polymers by Initial Layer Deposition before Plasma Etching

PLASMA PROCESSES AND POLYMERS, Issue S1 2009
Irmina Wendling
Abstract The generation of nanostructures by initial layer deposition and plasma etching offers a simple and cost-effective method for imparting broadband anti-reflection properties to polymer optics. In this study, we have investigated the possibility of controlling the structure growth on the cycloolefin polymer Zeonex®. It has been found that the geometry of the emerging nanostructures can be adjusted from "island-like," through "sponge-like," to "pinholes" merely by changing the thickness of the initial layer before the etching step. However, not all structure types provided a satisfactory transmittance enhancement. Only when the initial layer thickness and the etching time were matched in such a way that a certain material/air filling factor range and a sufficient structure depth were obtained could an outstanding anti-reflection effect be realized. [source]

Direct high-performance liquid chromatographic separation of the enantiomers of venlafaxine and 11 analogs using amylose-derived chiral stationary phases

CHIRALITY, Issue 6 2009
Salvatore Caccamese
Abstract A direct liquid chromatographic enantioselective separation of venlafaxine and 11 analogs was obtained in the normal phase mode using Chiralpak AD. For some compounds, a comparison between the enantioseparation using coated and immobilized amylose tris(3,5-dimethylphenylcarbamate) chiral stationary phases (Chiralpak AD and Chiralpak IA, respectively) was made. The best separations were achieved on Chiralpak AD with ethanol as alcoholic modifier in a mobile phase made basic by DEA addition: separation factor ranges between 2.08 and 1.15 and resolution factor between 7.0 and 1.0. Using the same CSP and 2-propanol doped with TFA as acidic modifier, 10 compounds were enantioseparated with separation factor ranging between 1.40 and 1.04 and resolution factor between 3.1 and 0.3. The use of ethanol as alcoholic modifier also has the advantage of better solubility of the compounds in the mobile phase. The nature of the substituent (electron donating or withdrawing) affects in general the separation factor. A memory effect that involves a long equilibration time of the CSP is present when switching from an acidic mobile phase to a basic one. Chirality, 2008. © 2009 Wiley-Liss, Inc. [source]