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Crosshead Speed (crosshead + speed)
Kinds of Crosshead Speed Selected AbstractsInfluence of contamination on resin bond strength to nano-structured alumina-coated zirconia ceramicEUROPEAN JOURNAL OF ORAL SCIENCES, Issue 4 2010Shanchuan Zhang Zhang S, Kocjan A, Lehmann F, Kosma, T, Kern M. Influence of contamination on resin bond strength to nano-structured alumina-coated zirconia ceramic. Eur J Oral Sci 2010; 118: 396,403. © 2010 The Authors. Journal compilation © 2010 Eur J Oral Sci The purpose of this study was to evaluate the influence of contamination and subsequent cleaning on the bond strength and durability of an adhesive resin to nano-structured alumina-coated zirconia ceramic. Zirconia ceramic disks were coated with nano-structured alumina, utilizing the hydrolysis of aluminum nitride powder. After immersion in saliva or the use of a silicone disclosing agent, specimens were cleaned with phosphoric acid etching or with tap water rinsing only. Uncontaminated specimens served as controls. Plexiglas tubes filled with composite resin were bonded with a phosphate monomer [10-methacryloxydecyl-dihydrogenphosphate (MDP)]-containing resin (Panavia 21). Subgroups of eight specimens each were stored in distilled water at 37°C, either for 3 d without thermal cycling (TC) or for 150 d with 37,500 thermal cycles from 5 to 55°C. The tensile bond strength (TBS) was determined using a universal testing machine at a crosshead speed of 2 mm min,1. The topography of the debonded surface was scrutinized for fractographic features, utilizing both optical and scanning electron microscopy. The TBS to uncontaminated nano-structured alumina-coated zirconia ceramic was durable, while contamination significantly reduced the TBS. Phosphoric acid cleaning was effective in removal of saliva contamination from the coated bonding surface but was not effective in removal of the silicone disclosing agent. Nano-structured alumina coating improves resin bonding to zirconia ceramic and eliminates the need for air-abrasion before bonding. [source] Enamel microhardness and bond strengths of self-etching primer adhesivesEUROPEAN JOURNAL OF ORAL SCIENCES, Issue 2 2010Olabisi A. Adebayo Adebayo OA, Burrow MF, Tyas MJ, Adams GG, Collins ML. Enamel microhardness and bond strengths of self-etching primer adhesives. Eur J Oral Sci 2010; 118: 191,196. © 2010 The Authors. Journal compilation © 2010 Eur J Oral Sci The aim of this study was to determine the relationship between enamel surface microhardness and microshear bond strength (,SBS). Buccal and lingual mid-coronal enamel sections were prepared from 22 permanent human molars and divided into two groups, each comprising the buccal and lingual enamel from 11 teeth, to analyze two self-etching primer adhesives (Clearfil SE Bond and Tokuyama Bond Force). One-half of each enamel surface was tested using the Vickers hardness test with 10 indentations at 1 N and a 15-s dwell time. A hybrid resin composite was bonded to the other half of the enamel surface with the adhesive system assigned to the group. After 24 h of water storage of specimens at 37º°C, the ,SBS test was carried out on a universal testing machine at a crosshead speed of 1 mm min,1 until bond failure occurred. The mean ,SBS was regressed on the mean Vickers hardness number (VHN) using a weighted regression analysis in order to explore the relationship between enamel hardness and ,SBS. The weights used were the inverse of the variance of the ,SBS means. Neither separate correlation analyses for each adhesive nor combined regression analyses showed a significant correlation between the VHN and the ,SBS. These results suggest that the ,SBS of the self-etch adhesive systems are not influenced by enamel surface microhardness. [source] Micro-shear bond strengths and etching efficacy of a two-step self-etching adhesive system to fluorosed and non-fluorosed enamelEUROPEAN JOURNAL OF ORAL SCIENCES, Issue 2 2009Kanako Shida The purpose of this study was to evaluate the micro-shear bond strengths and the etching efficacy of a two-step self-etching adhesive system to fluorosed and non-fluorosed enamel. The extracted teeth, obtained from Australian and Japanese patients, were classified according to the severity of fluorosis, using the Thylstrup & Fejerskov index (TFI). Australian teeth were classified as mildly fluorosed (TFI = 1,3), whereas Japanese teeth were classified as non-fluorosed (TFI = 0). Resin composite was bonded to 20 enamel samples using Clearfil SE bond. The bonded samples were stressed at a crosshead speed of 1 mm min,1 to determine the micro-shear bond strength. To examine the etching efficacy of primer on fluorosed and non-fluorosed enamel, the enamel-surface pH values were directly measured using a micro pH sensor. The non-fluorosed enamel showed significantly higher bond strengths compared with the fluorosed enamel. There was a statistical difference between fluorosed and non-fluorosed enamel regarding the surface pH change before and after application of the Clearfil SE bond primer. The results from this study suggest that water fluoridation has an effect on the acid resistance of enamel surfaces when treated with a two-step self-etching adhesive system and that this effect leads to reduced bond strengths. [source] Seven-year dentin bond strengths of a total- and self-etch systemEUROPEAN JOURNAL OF ORAL SCIENCES, Issue 3 2005Michael F. Burrow The aim of this study was to determine the durability of tensile bond strengths of a conventional 3-step bonding system (Superbond D-liner Plus) and a self-etching priming bonding system (Clearfil Liner Bond II) to bovine dentin over a 7 yr period. Superficial bovine dentin finished with 600-grit SiC paper was bonded with one of the two adhesive materials. A 4 mm diameter area was bonded, covered with resin composite and stored in 37°C deionized water containing gypsum chips and 0.4% sodium azide as an antibacterial. Bonds were stressed in tension at a crosshead speed of 1 mm min,1. Mean bond strengths were observed at 1 d, at 1, 3, and 6 months, and at 1, 2, 3, 6 and 7 yr. Ten specimens were tested for the first 3 yr and 15 specimens were tested for 6 and 7 yr. The bond strength of Superbond D-liner Plus significantly decreased over the 7 yr period, whereas Liner Bond II showed a slight but, insignificant, decrease. The fracture mode changed with time for Superbond D-liner Plus, but not for Liner Bond II. It was concluded that systems which use a strong acid for demineralizing the dentin may show greater deterioration of the bond to dentin compared with a self-etching priming system. [source] Fracture strength of bovine incisors after intra-radicular treatment with MTA in an experimental immature tooth modelINTERNATIONAL ENDODONTIC JOURNAL, Issue 9 2007E. A. Bortoluzzi Abstract Aim, To evaluate, using an experimental immature tooth model, the fracture resistance of bovine incisors submitted to different reinforcement treatments with mineral trioxide aggregate (MTA). Methodology, An immature tooth model was created by sectioning the coronal and apical portions of 40 bovine incisors 8 mm above and 12 mm below the cementoenamel junction. The root canals were irrigated with 1.0% sodium hypochlorite. They were enlarged both coronally and apically using number 703 carbide burs (ISO: 500,104-168-007-021) and their internal diameter was standardized to 2.1 mm. The specimens were assigned to four groups (n = 10): GI-control (without filling); GII-apical MTA plug + filling with gutta-percha and endodontic sealer; GIII-filling with MTA; GIV-apical MTA plug + filling with MTA + metallic post (Reforpost I). A polyether impression material was used to simulate the periodontal ligament. The specimens were submitted to a compressive load at a crosshead speed of 0.5 mm min,1 in a servo-hydraulic universal testing machine (MTS 810) applied at 45° to the long axis of the tooth until failure. Data were submitted to statistical analysis by the Kruskal,Wallis test at 5% significance level. Results, GIV presented the highest fracture resistance (32.7N) and differed significantly from the other groups (P < 0.05). No statistically difference was found between GII (16.6N) and GIII (23.4N) (P > 0.05). GIII had a significantly higher fracture resistance than GI (P < 0.05). Conclusions, The use of MTA + metallic post as an intra-radicular reinforcement treatment increased the resistance to fracture of weakened bovine teeth in an experimental immature tooth model. [source] Effect of curing mode on bond strength of self-adhesive resin luting cements to dentinJOURNAL OF BIOMEDICAL MATERIALS RESEARCH, Issue 1 2010T. R. Aguiar Abstract In this study, the in vitro bond strength of dual-curing resin cements to indirect composite restorations when the cement was either light polymerized or allowed to only autopolymerize was evaluated. Occlusal dentin surfaces of 56 extracted human third molars were flattened to expose coronal dentin. Teeth were assigned to eight groups (n = 7) according to resin cement products and polymerization modes: conventional cement (Panavia F 2.0; Kuraray Medical) and self-adhesive cements [RelyX Unicem (3M ESPE), BisCem (Bisco), and G-Cem (GC Corp.)]. Cements were applied to prepolymerized resin discs (2-mm-thick Sinfony; 3M ESPE), which were subsequently bonded to the prepared dentin surfaces. The restored teeth were either light-polymerized through the overlying composite according to manufacturers' instructions or were allowed to only self-cure. After 24 h, the teeth and restorations were sectioned to obtain multiple bonded beams (1.0 mm2) and tested in tension at a crosshead speed of 0.5 mm/min until failure. Data (MPa) were analyzed by two-way ANOVA and Tukey test (, = 0.05). Light activation of some cement systems (G-Cem and Panavia F 2.0) increased the bond strength, while the curing mode did not affect the bond strength for some (RelyX Unicem and BisCem). The bond strength in the autopolymerized mode varied among products. In general, the use of self-adhesive resin cements did not provide significantly higher bond strengths than that of a conventional material, and two self-adhesive cements yielded significantly lower bond values (regardless of cure mode) than the other products. © 2010 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 2010 [source] Bonding characteristics of newly developed all-in-one adhesivesJOURNAL OF BIOMEDICAL MATERIALS RESEARCH, Issue 2 2007S. K. Sidhu Abstract This study evaluated the microtensile bond strength and the interfacial morphology of newer adhesives. The occlusal surfaces of extracted teeth were ground flat for random allocation to four equal groups. Resin composite was bonded to each surface using either Clearfil SE Bond [SEB], Clearfil Protect Bond [PB], G-Bond [GB], or an experimental adhesive, SSB-200 [SSB]. After storage for 24 h in water at 37°C, they were sectioned into beams (cross-sectional area 1 mm2) for microtensile bond strength testing (,TBS) at a crosshead speed of 1 mm/min. The load at failure of each was recorded; the data were analyzed by one-way ANOVA and Games Howell tests. The surfaces of the fractured specimens were observed using SEM. For the ultra-morphology of the interface, the occlusal surfaces of four more teeth were prepared as before and a thin layer of flowable resin composite was bonded to each surface using one of the four adhesives. The mean ,TBS ranged from 39.68 MPa (GB) to 64.97 MPa (SEB). There were no statistical differences between SEB and SSB, or between PB and GB (p > 0.05). The ,TBS of SEB and SSB were significantly greater than that of PB and GB (p < 0.05). SEMs of the fractured surfaces revealed a mixed (cohesive/interfacial) failure. TEM examination highlighted differences in the hybrid layer; SEB had a thicker layer than the others. In conclusion, the newer all-in-one adhesives produced a thin hybrid layer but varied in their bond strengths. The 2-step self-etching adhesives do not necessarily produce higher bond strengths than that of the all-in-one systems. © 2006 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 2007 [source] Application of crosslinkers to dentin collagen enhances the ultimate tensile strengthJOURNAL OF BIOMEDICAL MATERIALS RESEARCH, Issue 1 2007Ana Karina B. Bedran-Russo Abstract The stabilization of dentin collagen with biocompatible crosslinking agents may be of clinical importance to improve dentin bond strength. The present study aimed to evaluate the effect of three collagen crosslinking agents on the ultimate tensile strength (UTS) of undemineralized and demineralized dentin. Ten freshly extracted sound molars were sectioned into 0.5 × 0.5 mm2 thick beams. The beams were either demineralized or kept undemineralized. Then, specimens were subdivided into four groups according to treatments,PBS solution (control), 5% glutaraldehyde (GD), 0.5% proanthocyanidin PBS solution (PA), and 0.625% genipin PBS solution (GE). Specimens were kept in their respective solutions for either 4 or 40 h. To assess UTS, specimens were subjected to tensile forces at a crosshead speed of 1 mm/min. Statistical analysis was performed using two-way ANOVA and Fisher's PLSD test (p < 0.05). Statistically significant increases in UTS were observed for demineralized dentin after PA and GE dentin treatment, when compared with those of the control group. Dentin treated with GD showed no statistically significant differences in UTS when compared with that the control. Undemineralized dentin revealed no significant differences as compared to that of the control, regardless of the collagen crosslinkers. The application of two naturally occurring crosslinkers, i.e., PA and GE, to dentin collagen significantly improves UTS, indicating its potential value in restorative dentistry. © 2006 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 2007 [source] Joint properties of cast Fe-Pt magnetic alloy laser welded to gold alloysJOURNAL OF BIOMEDICAL MATERIALS RESEARCH, Issue 1 2006Ikuya Watanabe Abstract This study investigated the joint properties of a cast Fe-Pt magnetic alloy (Fe-36 at % Pt) laser welded to three gold alloys. The gold alloys used were ADA Type II and Type IV gold alloys, and an Ag-based (Ag-Au) gold alloy. Cast plates (0.5 × 3.0 × 10 mm) were prepared for each alloy. After the cast Fe-Pt plates were heat treated, they were butted against each of the three alloys and then laser welded with Nd:YAG laser at 200 V. Homogeneously welded specimens were also prepared for each alloy. Tensile testing was conducted at a crosshead speed of 1 mm/min. Failure load (N) and elongation (%) were recorded. After tensile testing, the fractured surfaces were examined with the use of SEM. The failure-load values of the group of alloys welded homogeneously were ranked in the order of: Ag-Au alloy > Type IV alloy > Type II alloy > Fe-Pt alloy. The Type IV alloy welded to Fe-Pt alloy had the highest failure-load value among the three alloys tested. The elongation results tended to follow a similar pattern. The results of this study indicated that Type IV gold alloy is a suitable alloy for metal frameworks to which cast Fe-Pt magnetic alloy is laser welded. © 2005 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 2006 [source] VISCOELASTICITY OF A SIMULATED POLYMER AND COMPARISON WITH CHICKPEA FLOUR DOUGHSJOURNAL OF FOOD PROCESS ENGINEERING, Issue 3 2006NIDHI YADAV ABSTRACT An integrated approach consisting of compression and stress relaxation is performed with a simulated model system of poly dimethyl siloxane (PDMS), a viscoelastic polymer material when the compressive strain, height of sample and crosshead speed were varied. The parameters derived are the forces at the end of compression and relaxation, energy for compression and the extent of elasticity of the sample based on the ratios of forces as well as the proposed energy values. The results were verified with food doughs undergoing large deformations that show a nonlinear behavior. The proposed extent of elasticity based on the ratios of energy stored and compression can be used as an index for the characterization of viscoelasticity. A nonlinear three-parameter model had also been proposed to predict the stress decay characteristics as a function of time, which was found suitable for the PDMS system, and was better than the two-parameter Peleg model as judged by lower variance values (0.0006,0.018 and 0.002,0.048, respectively). Further, an actual system of food doughs in the form of chickpea (Cicer arietinum L.) flour dough was used to verify the proposed model and viscoelastic index at different moisture contents (27,39%) subjected to compressive strains of 25,75%. The nonlinear relaxation characteristics of the food dough are sensitive to moisture content as well as to strain level. [source] Fracture strength of copy-milled and conventional In-Ceram crownsJOURNAL OF ORAL REHABILITATION, Issue 7 2001Jung-Won Hwang The purpose of this study was to compare the fracture resistance of copy-milled and conventional In-Ceram crowns. Four groups of 10 uniform sized all-ceramic anterior crowns were fabricated for this test: (1) In-Ceram Spinell (2) In-Ceram Alumina (3) Celay In-Ceram Spinell, and (4) Celay In-Ceram Alumina crowns. All specimens were cemented on stainless steel master die with resin cement and stored in 37 °C water for one day prior to loading into a universal testing machine. Using a steel ball at a crosshead speed of 0·5 mm min,1, the crowns were loaded at 30 °C angle until catastrophic failure occurred. Mean fracture strength was analysed and compared. Under the conditions of this study and the materials used, the following conclusions were drawn: 1. The strength of Celay In-Ceram anterior crowns had a slightly higher fracture strength than conventional In-Ceram crowns. 2. In-Ceram Alumina crowns had a significantly higher fracture strength than In-Ceram Spinell crowns in both conventional and copy milling methods. [source] Effect of three adhesive primers for a noble metal on the shear bond strengths of three resin cementsJOURNAL OF ORAL REHABILITATION, Issue 1 2001K. Yoshida The purpose of this study was to evaluate the durability and shear bond strengths of the different combinations of three adhesive primers and three resin cements to a silver,palladium,copper,gold (Ag,Pd,Cu,Au) alloy. The adhesive primers Alloy Primer® (AP), Metal PrimerII® (MPII) and Metaltite® (MT), and the resin cements BistiteII® (BRII), Panavia Fluoro Cement® (PFC) and Super-Bond C&B® (SB) were used. Two sizes of casting alloy disks were either non-primed or primed and cemented with each of the three resin cements. The specimens were stored in a 37 °C water bath for 24 h and then immersed alternately in 4 and 60 °C water baths for 1 min each for up to 100 000 thermal cycles. Shear mode testing at a crosshead speed of 0·5 mm/min was then performed. The application of MPII or MT was effective for improving the shear bond strength between each of the three resin cements and the Ag,Pd,Cu,Au alloy compared with non-primed specimens. However, when primed with MPII or MT and cemented with SB, the bond strength at 100 000 thermal cycles was significantly lower than that at thermal cycle 0. When primed with AP, the specimens cemented with BRII or PFC showed lower bond strength than non-primed specimens and failed at the metal,resin cement interface at 100 000 thermal cycles. On the other hand, AP was effective in enhancing the shear bond strength of SB to the Ag,Pd,Cu,Au alloy. The five combined uses of an adhesive metal primer and resin cement (combinations of MPII or MT and BRII or PFC and AP and SB) are applicable to the cementation of prosthodontic restorations without complicated surface modification of the noble alloy. [source] Effect of Net Fiber Reinforcement Surface Treatment on Soft Denture Liner Retention and LongevityJOURNAL OF PROSTHODONTICS, Issue 4 2010MPhil, Muhanad M. Hatamleh BSc Abstract Purpose: To evaluate shear bond strength of Molloplast-B soft liner attached to different acrylic surfaces (smooth, rough, and Sticktech net fiber-reinforced interfaces) after 3000 thermal cycles. Materials and Methods: Sixty-nine specimens were fabricated by attaching Molloplast-B soft liner to acrylic bases of three interfaces (n= 23); smooth (Group 1, control), rough (Group 2), and Sticktech net fiber-reinforced interface (Group 3). The specimens underwent 3000 thermocycles (5 and 55°C) before being subject to a shear bond test at 2 mm/min crosshead speed. Debonding sites were investigated using an optical microscope at 40× magnification. Bond failures were categorized as adhesive, cohesive, or mixed. Results: Mean (SD) bond strength values (MPa) were: 0.71 (0.15); 0.63 (0.07); and 0.83 (0.12) for smooth, rough, and fiber-reinforced acrylic interfaces, respectively. The mean values were analyzed using one-way ANOVA and Bonferroni post hoc test for pairwise comparisons (p, 0.05). The net fiber-reinforced acrylic interface exhibited a statistically significantly higher bond strength value when compared to smooth and rough acrylic interfaces (P= 0.003 and P= 0.000, respectively). Modes of failure were mainly cohesive (91%), followed by mixed failures (9%). Conclusions: Molloplast-B exhibited a stronger bond to StickTech Net fiber-reinforced surfaces when compared to smooth and rough acrylic interfaces after thermocycling. This may enhance prosthesis serviceability during clinical use. [source] The Retention of Cast Metal Dowels Fabricated by Direct and Indirect TechniquesJOURNAL OF PROSTHODONTICS, Issue 1 2010MDentSci, Wael M. Al-Omari BDS Abstract Purpose: To explore the effect of fabrication technique, cement type, and cementation procedure on retention of cast metal dowels. Methods and Materials: Eighty intact single-rooted teeth were selected. The clinical crown was removed at the cementoenamel junction level. Each root was prepared to receive a cast metal dowel of 10-mm length and 1.45 mm in diameter. The 80 specimens were divided into two major groups of 40 based on fabrication technique (direct and indirect). Each group was further divided into four subgroups of ten based on the cement type (zinc phosphate and glass ionomer), and cementation procedure (with and without lentulo spiral). The dowels were subjected to a constantly increasing tensile force, in a universal Instron testing machine, at crosshead speed of 5 mm/min until failure. Results: The most significant factor to affect retention was the cementation procedure, as cementation with lentulo spiral produced greater retention than cementation without the use of lentulo spiral (p < 0.05); however, there seems to be a close interaction between fabrication technique, cement type, and cementation procedure (p= 0.051). The least retentive group was the one fabricated by direct technique, cemented with zinc phosphate without the use of lentulo spiral. Conclusion: Fabrication technique does not affect retention of cast dowels, except when zinc phosphate was the luting agent and placed in the canal space without using a lentulo spiral. The cementation procedure had a significant effect on retention; thus, it is recommended that cementation should be done using the lentulo spiral. [source] Evaluation of the Bond Strength of Denture Base Resins to Acrylic Resin Teeth: Effect of ThermocyclingJOURNAL OF PROSTHODONTICS, Issue 5 2009Juliê Marra DDS Abstract Purpose: The purpose of this study was to evaluate the thermocycling effects and shear bond strength of acrylic resin teeth to denture base resins. Materials and Methods: Three acrylic teeth (Biotone, Trilux, Ivoclar) were chosen for bonding to four denture base resins: microwave-polymerized (Acron MC), heat-polymerized (Lucitone 550 and QC-20), and light-polymerized (Versyo.bond). Twenty specimens were produced for each denture base/acrylic tooth combination and were divided into two groups (n = 10): without thermocycling (control groups) and thermocycled groups submitted to 5000 cycles between 4 and 60°C. Shear strength tests (MPa) were performed with a universal testing machine at a crosshead speed of 1 mm/min. Statistical analysis of the results was carried out with three-way ANOVA and Bonferroni's multiple comparisons post hoc analysis for test groups (,= 0.05). Results: The shear bond strengths of Lucitone/Biotone, Lucitone/Trilux, and Versyo/Ivoclar specimens were significantly decreased by thermocycling, compared with the corresponding control groups (p < 0.05). The means of Acron/Ivoclar and Lucitone/Ivoclar specimens increased after thermocycling (p < 0.05). The highest mean shear bond strength value was observed with Lucitone/Biotone in the control group (14.54 MPa) and the lowest with QC-20/Trilux in the thermocycled group (3.69 MPa). Conclusion: Some acrylic tooth/denture base resin combinations can be more affected by thermocycling; effects vary based upon the materials used. [source] Fracture Resistance of Endodontically Treated Teeth: Three Walls versus Four Walls of Remaining Coronal Tooth StructureJOURNAL OF PROSTHODONTICS, Issue 1 2009Siriporn Arunpraditkul DDS Abstract Purpose: The purpose of this study was to evaluate the fracture resistance of endodontically treated teeth between those with four walls and those with three walls of remaining coronal tooth structure and the effect of the site of the missing coronal wall. Materials and Methods: Thirty-two endodontically treated second mandibular premolars were decoronated, leaving 3 mm above the cementoenamel junction (CEJ). A 0.5-mm-wide chamfer was prepared 1 mm above the CEJ. The teeth were randomly divided into four groups. Group 1 had four walls of coronal tooth structure, whereas groups 2, 3, and 4 had only three walls, missing the buccal, lingual, and mesial wall, respectively. The cast dowel and cores and crowns (Ni,Cr alloy) were cemented with zinc phosphate cement. A compressive load was applied 45° to the long axis, 2 mm below the buccal cusp, with an Instron machine until failure at a crosshead speed of 5 mm/min. Failure load (kg) and mode of failure were recorded. Data were analyzed with one-way ANOVA and Scheffé tests (p < 0.05). Results: Group 1 had the highest fracture resistance (1190.3 ± 110.5 kg), significantly different from the other groups (p < 0.05) (group 2: 578.5 ± 197.4 kg; group 3: 786.6 ± 132.8 kg; group 4: 785.4 ± 289.9 kg). There were no significant differences among the test groups. The mode of failure in group 1 was a horizontal root fracture, whereas that of the other groups was either vertical or oblique fracture. Conclusions: Teeth with four walls of remaining coronal dentine had significantly higher fracture resistance than teeth with only three walls. The site of the missing coronal wall did not affect the fracture resistance of endodontically treated teeth. [source] Effect of Aluminum Oxide Addition on the Flexural Strength and Thermal Diffusivity of Heat-Polymerized Acrylic ResinJOURNAL OF PROSTHODONTICS, Issue 6 2008Ayman E. Ellakwa BDS Abstract Purpose: This work was undertaken to investigate the effect of adding from 5% to 20% by weight aluminum oxide powder on the flexural strength and thermal diffusivity of heat-polymerized acrylic resin. Materials and Methods: Seventy-five specimens of heat-polymerized acrylic resin were fabricated. The specimens were divided into five groups (n = 15) coded A to E. Group A was the control group (i.e., unmodified acrylic resin specimens). The specimens of the remaining four groups were reinforced with aluminum oxide (Al2O3) powder to achieve loadings of 5%, 10%, 15%, and 20% by weight. Specimens were stored in distilled water at 37°C for 1 week before flexural strength testing to failure (5 mm/min crosshead speed) in a universal testing machine. Results were analyzed by one-way analysis of variance and post hoc Tukey paired group comparison tests (p < 0.05). Weibull analysis was used to calculate the Weibull modulus, characteristic strength, and the required stress for 1% and 5% probabilities of failure. Cylindrical test specimens (5 specimens/group) containing an embedded thermocouple were used to determine thermal diffusivity over a physiologic temperature range (0 to 70°C). Results: The mean flexural strength values of the heat-polymerized acrylic resin were (in MPa) 99.45, 119.92, 121.19, 130.08, and 127.60 for groups A, B, C, D, and E, respectively. The flexural strength increased significantly after incorporation of 10% Al2O3. The mean thermal diffusivity values of the heat-polymerized acrylic resin (in m2/sec) were 6.8, 7.2, 8.0, 8.5, and 9.3 for groups A, B, C, D, and E, respectively. Thermal diffusivities of the composites were found to be significantly higher than the unmodified acrylic resin. Thermal diffusivity was found to increase in proportion to the weight percentage of alumina filler, which suggested that the proper distribution of alumina powders through the insulating polymer matrix might form a pathway for heat conduction. Conclusion: Al2O3 fillers have potential as added components in denture bases to provide increased flexural strength and thermal diffusivity. Increasing the flexural strength and heat transfer characteristics of the acrylic resin base material could lead to more patient satisfaction. [source] Cement Selection for Cement-Retained Crown Technique with Dental ImplantsJOURNAL OF PROSTHODONTICS, Issue 2 2008James L. Sheets DDS Abstract Purpose: The purpose of this study was to assess and compare the retentive nature of common dental cements that have been adapted for use in the implant abutment cement-retained crown (CRC) technique with those specifically formulated for this purpose. Materials and Methods: Ten regular diameter implant analogs were embedded in stainless steel disks. Unmodified CRC abutments were attached and torqued to 30 Ncm. Test crowns were waxed and cast with base metal alloy. Castings were fitted, cleaned with aluminum oxide, and steam cleaned prior to application of the cement. The cements used were: (1) Temp Bond, (2) UltraTemp, regular, (3) UltraTemp firm, (4) ImProv with petroleum jelly coating of crown, (5) ImProv without petroleum jelly, (6) Premier Implant with KY Jelly coating of abutment, (7) Premier Implant without KY jelly, (8) TR-2, (9) Fleck's, (10) Ketac Cem Aplicap, and (11) Fuji Plus Capsule. After cementation, assemblies were stored for 24 hours. Each sample was subjected to a pull-out test using an Instron universal testing machine at a crosshead speed of 5.0 mm/min. Loads required to remove the crowns were recorded, and mean values for each group determined. A one-way ANOVA and a post hoc least square difference (LSD) test were done for pairwise comparison at a confidence interval of 95%. Results: The mean values (±SD) of loads at failure (n = 10) for various cements were as follows (N): Ultratemp, regular 358.6 (±38.2) (Group A), ImProv without petroleum jelly 172.4 (±59.6) (Group B), Fleck's 171.8 (±62.2) (Group B), Ketac Cem 167.8 (±69.1) (Group B), UltraTemp firm 158.8 (±62.7) (Group BC), Fuji Plus 147.5 (±69.7) (Group BC), Premier without KY jelly 131.6 (±31.8) (Group BC), ImProv using petroleum jelly 130.8 (±42.5) (Group BC), Temp Bond 117.8 (±48.3) (Group C), TR-2 41.2 (±16.6) (Group D), and Premier with KY jelly 31.6 (±24.8) (Group D). Groups with the same letter were not significantly different. Conclusions: Within the limitations of this in vitro study, it is not suggested that any one cement is better than another at retaining cement-retained crowns (CRCs) to implant abutments or that a threshold value must be accomplished to ensure retention. The ranking of cements presented is meant to be a discretionary guide for the clinician in deciding the amount of desired retention between castings and implant abutments. [source] The Effect of Denture Cleansing Solutions on the Retention of Yellow Hader Clips: An In Vitro StudyJOURNAL OF PROSTHODONTICS, Issue 3 2007Reena M. Varghese DMD Purpose: To evaluate the retention of yellow Hader clips after exposure to various denture cleansers. Methods: Seven groups of 18 yellow Hader clips each were soaked for the equivalent of 6 months of clinical use in the following denture cleansing solutions: Polident Regular, Polident Overnight, Efferdent, 5.25% Sodium Hypochlorite (NaOCl, 1:10 dilution) 15 min/day, NaOCl (1:10 dilution) 8 hours/day, water and dry (control) group. A Universal Testing Machine, set at a crosshead speed of 2 in/min, pulled each clip once, and the peak load-to-dislodgement was recorded and used as a measure to reflect changes in the retention of the Hader clips. Data were analyzed by a one-way analysis of variance followed by Tukey's HSD test. A p value , 0.05 was considered significant. Results: Denture cleansing solutions affected the retentive values of yellow Hader clips (F= 6.102, p, .0001). Sodium hypochlorite solution, 15 min/day for 6 months, caused an increase in the retentive values of the clips tested with a mean peak load-to-dislodgement of 22.63 ± 1.29 N. In addition, clips soaked in water showed no difference in retentive values when compared with all other groups. Furthermore, Polident Regular, Polident Overnight, Efferdent, and NaOCl (8 hours/day) had no effect on the retentive values of yellow Hader clips. Conclusion: This in vitro study demonstrated that the retention of yellow Hader clips used in implant overdentures is unaffected when soaked in commercial effervescent denture cleansers (Polident 5 Minute, Polident Overnight, and Efferdent) for six simulated months. Sodium hypochlorite statistically increased the single-pull retentive values of the clips, an effect that may not be beneficial. Increased retentive values may be associated with reduced durability of clips; further research is needed to address this issue. [source] An In Vitro Investigation of a Comparison of Bond Strengths of Composite to Etched and Air-Abraded Human Enamel SurfacesJOURNAL OF PROSTHODONTICS, Issue 1 2006G.B. Gray BDS Purpose: The purposes of the study were to measure the tensile bond strength of composite resin to human enamel specimens that had been either etched or air-abraded, and to compare the quality of the marginal seal, through the assessment of microleakage, of composite resin to human enamel specimens that had been either etched or air-abraded. Materials and Methods: Thirty mandibular molar teeth were decoronated and sectioned mesio-distally to produce six groups, each containing ten specimens that were embedded in acrylic resin using a jig. In each of the four treatment groups, the specimen surfaces were treated by either abrasion with 27 or 50 ,m alumina at 4 mm or 20 mm distance, and a composite resin was bonded to the treated surfaces in a standardized manner. In the two control groups the specimens were treated with 15 seconds exposure to 36% phosphoric acid gel and then similarly treated before being stored in sterile water for 1 week. All specimens were then subjected to tensile bond strength testing at either 1 or 5 mm/min crosshead speed. For the microleakage study, the degree of dye penetration was measured 32 times for each treatment group, using a neutral methylene blue dye at the interface between composite and either 27 or 50 ,m air-abraded tooth structure or etched enamel surfaces. Results: The mean bond strength values recorded for Group 1 (phosphoric acid etch, 5 mm/min crosshead speed) was 25.4 MPa; Group 2 (phosphoric acid etch, 1 mm/min), 22.2 MPa; Group 3 (27 ,m alumina at 4 mm distance), 16.8 MPa; Group 4 (50 ,m alumina at 4 mm distance), 16.9 MPa; Group 5 (27 ,m alumina at 20 mm distance), 4.2 MPa; and for Group 6 (50 ,m alumina at 20 mm distance) 3.4 MPa. An analysis of variance (ANOVA) demonstrated significant differences among the groups, and a multiple comparison test (Tukey) demonstrated that conventionally etched specimens had a greater bond strength than air-abraded specimen groups. No significant difference in dye penetration could be demonstrated among the groups (p= 0.58). Conclusions: Composite resin applied to enamel surfaces prepared using an acid etch procedure exhibited higher bond strengths than those prepared with air abrasion technology. The abrasion particle size did not affect the bond strength produced, but the latter was adversely affected by the distance of the air abrasion nozzle from the enamel surface. The crosshead speed of the bond testing apparatus had no effect on the bond strengths recorded. The marginal seal of composite to prepared enamel was unaffected by the method of enamel preparation. [source] Fracture Resistances of Cast Metal and Ceramic Dowel and Core Restorations: A Pilot StudyJOURNAL OF PROSTHODONTICS, Issue 2 2005Emine Yalç, n DDS Purpose: The purpose of this study was to compare fracture strengths of teeth restored with cast metal and ceramic dowel and cores supporting all-ceramic crowns. Materials and Methods: Eighteen recently extracted teeth were randomly divided into 3 equal groups. Metal dowel and cores (MDC) were fabricated for 1 group using a base metal alloy, and served as the control. The other groups received In-Ceram Spinell® (ICS) and IPS Empress 2® (IPS) dowel and cores. IPS Empress 1 crowns were fabricated for all samples. Each tooth was subjected to a shear force at a crosshead speed of 2 mm/min on a universal testing machine until failure occurred. Results: The mean fracture strengths and standard deviations of MDC, ICS, and IPS restorations were 1101 N (361), 832 N (288), and 1137 N (367), respectively. The differences between groups were insignificant (p < 0.05). Fractures of the all-ceramic crowns were observed in the MDC group, whereas the failure of ceramic dowel and core restorations was associated with root fracture at the cervical region. Conclusions: Due to improved mechanical properties, In-Ceram Spinell® and IPS Empress 2® ceramic dowel and cores may be candidates for the restoration of endodontically treated anterior teeth. [source] SENSORY AND INSTRUMENTAL TEXTURE MEASUREMENT OF THERMALLY PROCESSED RICEJOURNAL OF SENSORY STUDIES, Issue 5 2005M. PRAKASH ABSTRACT Rice is the staple food of many countries and its sensory quality is of great concern to the consumers. Its preservation through thermal processing in retort pouches for ready-to-eat purposes was carried out by different time,temperature schedules with and without oil to achieve a minimum Foof 3 min. The sensory analysis of the cooked rice carried out using quantitative descriptive analysis showed that a process schedule of 118C, 8 min was optimum to have the optimal sensory characteristics. The same rice samples were subjected to instrumental texture measurements by texture analyzer using a crosshead speed of 0.5 mm/s with 90% compression for hardness and stickiness parameters. The instrumental hardness showed high correlation with sensory hardness, chewiness and overall quality (r = 0.72; r = 0.73; r = 0.79) and a negative correlation with sensory stickiness (r = ,0.75). Applying principal component analysis, thermally processed rice samples were further classified based on the sensory and instrumental texture attributes. [source] TEXTURE PROFILE ANALYSIS , HOW IMPORTANT ARE THE PARAMETERS?JOURNAL OF TEXTURE STUDIES, Issue 5 2010ANDREW J. ROSENTHAL ABSTRACT A starch-glycerol gel was subjected to a two-bite compression test using two sample-instrument geometries, various speeds of compression and strain levels, both with lubrication or not. Results were interpreted using the primary characteristic terminology previously defined in Texture Profile Analysis. Compression speeds from 0.1 to 10 m/s showed a logarithmic relationship with hardness, cohesiveness, corrected cohesiveness and adhesiveness. Gels survived compression to strains of 0.90 without failing, strain levels from 0.25 to 0.90 resulted in an exponential rise in hardness with increasing strain and linear reduction in corrected cohesiveness. Lubrication had no significant influence on any of the measured parameters and an application of force with different sample-instrument geometry revealed that parallel plates and plungers only had an influence on gel hardness. Caution is urged when researchers modify the test protocol from 75% deformation with parallel plates. A minimum crosshead speed of 2 mm/s is recommended. PRACTICAL APPLICATIONS Texture Profile Analysis has been widely applied to test solid and semisolid foods; however, some researchers deviate from the original test protocol. This article attempts to show how modifying the parameters in the test protocol can influence the apparent properties of the sample. [source] Shear bond strength of luting agents to fixed prosthodontic restorative core materialsAUSTRALIAN DENTAL JOURNAL, Issue 4 2009N Capa Abstract Background:, Bonding properties of luting cements are important for retention of restorative core materials. The aim of this study was to compare the bonding performance of a resin-modified glass ionomer cement and a self-adhesive resin cement to various fixed prosthodontic core materials. Methods:, Cylindrical specimens with a thickness of 2 mm and a diameter of 5 mm were fabricated from Au-Pd-Ag, Co-Cr, Ni-Cr-Mo, Ni-Cr-Fe alloys, titanium, zirconia and Empress II (n = 20). Each group was divided into two subgroups to be luted with two different luting agents. Composite resin blocks were cemented onto specimens with RelyXUnicem and FujiCem. A shear bond strength machine with 50 kg load cell and 0.50 mm/min crosshead speed was used. Kruskal Wallis test, Dunn's Multiple Range test and Mann-Whitney-U test were used for statistical analysis. The results were evaluated in a confidence interval of p < 0.05. Results:, The highest bond strength was obtained between Ni-Cr-Fe-RelyXUnicem (8.22 ± 2.15 MPa) and the lowest was between Empress II-FujiCem (1.48 ± 0.9 MPa). In FujiCem groups, Co-Cr and Ni-Cr-Fe showed significantly higher bond strength than Au-Pd-Ag and Empress II. In RelyX Unicem groups, Ni-Cr-Fe showed higher bond strength than Empress II. Conclusions:, The types of luting agents and restorative core materials may have a significant influence on bond strength. [source] Improved Correlation Between Sensory and Instrumental Measurement of Peanut Butter TextureJOURNAL OF FOOD SCIENCE, Issue 5 2002C.M. Lee And Two commercial peanut butters and 3 laboratory-prepared peanut butters containing 0.5, 1.5 and 2.5% stabilizer were evaluated by sensory and instrumental texture profile analysis (TPA) using an Instron. A 2×3 factorial design consisting of crosshead speeds of 5 and 50 mm/min, and amount and type of fluid added was used. A descriptive panel (n= 11) was used to evaluate 14 sensory TPA attributes. Twelve sensory TPA attributes, compared with only 2 found by other researchers, were highly correlated ( 0.88) with 1 or more instrumental TPA parameters. Prediction models (R 0.71) developed successfully predicted 12 sensory texture attributes from instrumental TPA results. Eleven models, excluding surface roughness, were successfully verified with 0.74 to 7.21% error. [source] MEASUREMENT OF BITING VELOCITIES AT PREDETERMINED AND INDIVIDUAL CROSSHEAD SPEED INSTRUMENTAL IMITATIVE TESTS FOR PREDICTING SENSORY HARDNESS OF GELATIN GELSJOURNAL OF SENSORY STUDIES, Issue 2 2005M. FINNEY ABSTRACT Jaw movements during the act of biting were measured for seven subjects trained in descriptive analysis using an electrognathograph. The effectiveness of instrumental imitative tests performed at predefined and individual crosshead speeds (matching velocities measured in vivo) to predict the perception of hardness in 14 gelatin gels was assessed. For all seven subjects, the perception of hardness was adequately described by imitative instrumental tests performed with dental replicas of individual subjects (0.88 < R < 0.97). For some of the subjects, tests performed at crosshead speeds matching biting speeds improved the instrumental prediction of hardness, suggesting that biting velocity is an important aspect of the perception of hardness in food. [source] MEASUREMENT OF BITING VELOCITIES, AND PREDETERMINED AND INDIVIDUAL CROSSHEAD SPEED INSTRUMENTAL IMITATIVE TESTS FOR PREDICTING CHEESE HARDNESSJOURNAL OF TEXTURE STUDIES, Issue 1 2002J.-F. MEULLENET ABSTRACT Average first bite velocities of ten cheeses were measured for seven subjects trained in descriptive analysis using an electrognathograph. The effectiveness of instrumental imitative tests performed at predefined and individual crosshead speeds (matching velocities measured in vivo) to predict hardness perception of cheeses were assessed. For five of the seven subjects, the perception of hardness was adequately described by imitative instrumental tests performed with dental replicas of individual subjects. For some of the subjects (2 of 5), individual crosshead speed testing significantly improved the instrumental prediction of hardness. For other subjects, the instrumental test method did not seem to greatly influence the results. [source] | |||||||||||||