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Resin Interface (resin + interface)
Selected AbstractsInter-crystallite nanoretention of self-etching adhesives at enamel imaged by transmission electron microscopyEUROPEAN JOURNAL OF ORAL SCIENCES, Issue 6 2002Matthias Hannig The purpose of this in vitro study was to analyse the mode of action of self-etching adhesive systems when applied for resin-to-enamel bonding. Transmission electron microscopy was used to investigate the enamel,resin interface after application of non-rinsing self-etching adhesive systems based on phosphoric acid estered methacrylates (Clearfil Liner Bond 2, Clearfil SE Bond, Etch & Prime 3.0 and Resulcin AquaPrime) compared with conventional phosphoric acid etching and bonding (Heliobond). Non-decalcified ultrathin sections from the interface between enamel and self-etching adhesive systems revealed a 1.5,3.2-µm deep enamel surface layer characterized by a less-dense arrangement of enamel crystallites separated from each other by nanometer-sized spaces. A 1.5,3.2-µm wide, netlike resinous structure was observed in corresponding decalcified specimens, indicating that self-etching priming agents dissolve the peripheral and central part of the enamel crystallites, while simultaneously promoting inter- and intra-crystallite monomer infiltration. A similar pattern, but greater depth (6.9 µm) of enamel surface hybridization was found in the phosphoric acid-etched and bonded specimens. The nanoretentive interlocking between enamel crystallites and resin could explain the potential of self-etching adhesive systems in resin-to-enamel bonding despite the less distinct enamel etching pattern observed in scanning electron microscopy investigations. [source] Effect of Aging on Coronal Microleakage in Access Cavities through Metal Ceramic Crowns Restored with Resin CompositesJOURNAL OF PROSTHODONTICS, Issue 5 2010Ali Abdullah Alwan Al-Maqtari BDS Abstract Purpose: The purpose of this in vitro study was to determine if packable resin composite with/without flowable resin composite has the ability to prevent coronal leakage in restored endodontic access openings following aging. Materials and Methods: Eighty simulated standardized access cavities of metal-ceramic crowns were fabricated and fixed on Vitrebond cavities filled with an epoxy resin. The specimens were randomly divided into two main groups: (1) Group A,Access cavities filled with only packable composite (Filtek P60); (2) Group B,Access cavities filled with Filtek P60 and a flowable composite (Filtek Z350) as liner. Each main group was further subdivided randomly into four subgroups according to water storage and thermocycling periods. All specimens were immersed in blue ink solution for 24 hours and then sectioned into quadrants. The extension of blue ink along the metal-ceramic crown/composite resin interface was measured linearly using image analyzer and then analyzed by three-way ANOVA and independent t -test with a Mann-Whitney test. The level of significance was set at p < 0.05. Results: All tested subgroups demonstrated different levels of microleakage. There was no significant difference related to restorative technique; however, there was a significant difference related to water storage and thermocycling. Conclusions: All tested techniques and materials in this study showed microleakage. Packable composite while a flowable liner showed a marginally better result than packable composite alone. Excessive thermocycling resulted in significant differences among the test groups. [source] Effect of Compromised Cortical Bone on Implant Load DistributionJOURNAL OF PROSTHODONTICS, Issue 8 2008vanç Akça DDS Abstract Purpose: To investigate photoelastically the difference in load distribution of dental implants with different implant neck designs in intact and compromised bone. Materials and Methods: Composite photoelastic models were fabricated using two different resins to simulate trabecular bone and a 1-mm thick layer of cortical bone. The following parallel-sided, threaded implants were centrally located in individual models representing intact and compromised cortical bone: Straumann (4.1-mm diameter × 12-mm length), AstraTech (4.0-mm diameter × 13-mm length), and 3i (3.75-mm diameter × 13-mm length). The compromised cortical bone condition was simulated by contaminating a 1-mm neck portion with Vaseline to impair the implant,resin interface. Vertical and oblique static loads were applied on the abutments, and the resulting stresses were monitored photoelastically and recorded photograhphically. Results: For the fully intact condition, the highest stresses were observed around the crest and apical region for all implant designs under vertical and inclined loads. There were no appreciable differences in magnitude or distribution between implant types. With compromised cortical bone, for all designs and load directions, higher stresses in the supporting structures were observed. Increased stresses were noted especially at the cortical bone,trabecular bone interface. Somewhat lower stress levels were observed with the 3i implant. Conclusions: The condition of implant,cortical bone contact has considerable influence on stress distribution. A compromised cortical bone condition caused higher level stresses for all implant designs tested. [source] Comparison of Repair Methods for Ceramic-Fused-to-Metal CrownsJOURNAL OF PROSTHODONTICS, Issue 5 2006Mutlu Özcan DMD Purpose: The objective of this study was to evaluate the effect of four repair methods on the fracture load of repaired ceramic-fused-to-metal crowns. Materials and Methods: Metal-ceramic crowns were fractured, and the failure load was measured. The fractured metal-ceramic crowns (n = 9) were assigned randomly to the following treatment groups: (1) hydrofluoric acid (9.5%) etching, (2) air-particle abrasion (50 ,m Al2O3), (3) silica coating (30 ,m SiOx), and (4) the application of a layer of glass fiber-reinforced composite (FRC) (thickness: 0.12 mm) on the repair surface. The crowns were repaired with a highly filled resin composite and subjected to 3 repair cycles (n = 27). All specimens were stored in water at 37°C for 24 hours and then thermocycled (6000 cycles, 5°C to 55°C). The fracture load values for final failure of intact and repaired crowns were measured with a universal testing machine, and failure types were recorded. Results: No significant differences ( p > 0.05) were found between the final failure values for the groups treated with 9.5% hydrofluoric acid (376 N) and airborne particle abrasion with either Al2O3 (432 N) or SiOx (582 N) followed by silanization, respectively. Significantly, higher ( p < 0.0001) final failure values (885 N) were obtained with the use of the FRC layer when compared with the other repaired groups. There was no significant difference ( p > 0.05) between the final fracture load of intact crowns (872 N) and those repaired with FRC (885 N) (One-way ANOVA with repeated measures, Bonferroni test). No significant difference in fracture loads was found between the 1st, 2nd, and 3rd repair cycles (558 N, 433 N, 485 N, respectively). Failure sites were predominantly at the alloy/veneering resin interface in Group 1; Groups 2 and 3 both showed more cohesive failures than Group 1. In the case of FRC, the failure pattern was exclusively cohesive between the two laminates of FRC layer. Conclusions: The conditioning methods (Groups 1 to 3) of the repair surfaces did not show differences between each other; each resulted in mean fracture loads at lower levels than that of the intact crowns. Addition of an FRC layer increased the fracture load to the level of intact crowns. This suggests that the use of FRC in repairs of metal-ceramic crowns might be a viable option. [source] Bonding to Zirconia Using a New Surface TreatmentJOURNAL OF PROSTHODONTICS, Issue 5 2010Moustafa N. Aboushelib DDS Abstract Purpose: Selective infiltration etching (SIE) is a newly developed surface treatment used to modify the surface of zirconia-based materials, rendering them ready for bonding to resin cements. The aim of this study was to evaluate the zirconia/resin bond strength and durability using the proposed technique. Materials and Methods: Fifty-four zirconia discs were fabricated and divided into three groups (n = 18) according to their surface treatment: as-sintered surface (control group), airborne-particle abrasion (50-,m aluminum oxide), and SIE group. The zirconia discs were bonded to preaged composite resin discs using a light-polymerized adhesive resin (Panavia F 2.0). The zirconia/resin bond strength was evaluated using microtensile bond strength test (MTBS), and the test was repeated after each of the following intervals of accelerated artificial aging (AA): thermocycling (10,000 cycles between 5 and 55°C), 4 weeks of water storage (37°C), and finally 26 weeks of water storage (37°C). Silver nitrate nanoleakage analysis was used to assess the quality of zirconia/resin interface. A repeated measures ANOVA and Bonferroni post hoc test were used to analyze the data (n = 18, ,= 0.05) Results: There were significant differences in the MTBS values between the three test groups at each of the test intervals (p < 0.001). AA resulted in reduction in the bond strength of the as-sintered and the particle-abraded groups (5.9 MPa and 27.4, MPa, respectively). Reduction in the bond strength of these groups was explained by the observed nanoleakage across the zirconia/resin interface. The bond strength of the SIE specimens was stable after completion of AA (51.9 MPa), which also demonstrated a good seal against silver nitrate penetration across the zirconia/resin interface. Conclusion: SIE established a strong, stable, and durable bond to zirconia substrates. Conservative resin-bonded zirconia restorations are now possible using this new technique. [source] | ||||||||||