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Terms modified by Rectangular Selected AbstractsCrescent Versus Rectangle: Is It a True Negative Margin in Second and Subsequent Stages of Mohs Surgery?DERMATOLOGIC SURGERY, Issue 2 2010YUE YU MD BACKGROUND The hallmark of Mohs micrographic surgery is using tangential tissue sections that theoretically allow 100% of the tissue margin to be examined, but when taking additional layers for second and subsequent Mohs stages, no detailed methods have been described to ensure that 100% of the tissue margins are analyzed. METHOD A rectangular or a crescent-shaped layer is often used to take second and subsequent stages. Here we compare the two techniques for their theoretic advantages and disadvantages. SUMMARY The advantage of the rectangular shape has been ease of processing, as well as built in vertical "nicks" that automatically mark the border of the tissue removed, but the rectangular layer may not provide 100% evaluation of the tumor margin because the vertical edges of the rectangular layer are not always completely analyzed, and thus tumor cells cannot be visualized in the vertical margins of these layers. This might result in a false-negative margin reading, which can be avoided by using the crescent layer. CONCLUSION We propose taking second and subsequent Mohs layers with only a crescent shape, which allows true 100% tissue margin assessment. The authors have indicated no significant interest with commercial supporters. [source] Intranuclear cytoplasmic inclusions in fine-needle aspiration smears of papillary thyroid carcinoma: A study of its morphological forms, association with nuclear grooves, and mode of formationDIAGNOSTIC CYTOPATHOLOGY, Issue 5 2005D.SC., Dilip K. Das M.B.B.S., Ph.D. Abstract Intranuclear cytoplasmic inclusion (INCI) and nuclear grooves in fine-needle aspiration (FNA) smears of papillary thyroid carcinoma (PTC) represent cytoplasmic invaginations into the nucleus. Although formation of INCIs is linked to nuclear grooves, they seldom exist together. This study was undertaken to find out the various morphological forms of INCIs, their relation to nuclear grooves, and mode of formation. FNA smears of 54 PTC cases were studied for various forms of INCI, nuclear chromatin pattern, nuclear grooves, and nuclear notches. A differential count of INCIs was made in 19 cases having ,10 INCIs per 200 neoplastic cells. INCIs were present in 48 (88.9%) of 54 PTC cases. Round INCIs were present in 46 (85.2%) cases, followed by oval (48.1%), tear drop/flask-shaped (18.5%), irregular (14.8%), planoconvex/semicircular (13%), rectangular (9.3%), spindle-shaped (3.7%), and bilobed (3.7%). A differential count of INCIs also showed that the round form was the commonest (76.3%). The oval and other forms constituted 19.5 and 4.2%, respectively. INCIs and nuclear grooves were present together in a cell in 15 (27.8%) cases. The formation of INCIs as a cytoplasmic invagination into the nucleus was shown cytomorphologically in rare cells. For the first time in this study, the various morphological forms of INCIs, and the extent of their coexistence with nuclear grooves, (have been highlighted) and showed their mode of formation shown at a light microscopic level. Diagn. Cytopathol. 2005;32:264,268. © 2005 Wiley-Liss, Inc. [source] Unnatural landscapes in ecology: generating the spatial distribution of brine spills,ENVIRONMETRICS, Issue 7 2005Henriette I. Jager Abstract Quantitative tools are needed to evaluate the ecological effects of increasing petroleum production. In this article, we describe two stochastic models for simulating the spatial distribution of brine spills on a landscape. One model uses general assumptions about the spatial arrangement of spills and their sizes; the second model distributes spills by siting rectangular well complexes and conditioning spill probabilities on the configuration of pipes. We present maps of landscapes with spills produced by the two methods and compare the ability of the models to reproduce a specified spill area. A strength of the models presented here is their ability to extrapolate from the existing landscape to simulate landscapes with a higher (or lower) density of oil wells. Published in 2005 by John Wiley & Sons, Ltd. [source] Hafnium Oxide Doped Mesostructured Silica FilmsEUROPEAN JOURNAL OF INORGANIC CHEMISTRY, Issue 18 2007Ralf Supplit Abstract Hafnium oxide doped silica films with ordered mesostructures were produced with hafnium:silicon ratios between 1:60 and 1:6. A surfactant,hafnium alkoxide complex was synthesized and used as a template in a sol,gel dip-coating process. Face-centred orthorhombic, 2D centred rectangular and lamellar films were formed by evaporation-induced self-assembly (EISA). The influence of subsequent heat treatment was studied by GISAXS and TEM. The surface and in-depth molecular composition of the films was studied by XPS.(© Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2007) [source] Comparison of methods to model the gravitational gradients from topographic data basesGEOPHYSICAL JOURNAL INTERNATIONAL, Issue 3 2006Christopher Jekeli SUMMARY A number of methods have been developed over the last few decades to model the gravitational gradients using digital elevation data. All methods are based on second-order derivatives of the Newtonian mass integral for the gravitational potential. Foremost are algorithms that divide the topographic masses into prisms or more general polyhedra and sum the corresponding gradient contributions. Other methods are designed for computational speed and make use of the fast Fourier transform (FFT), require a regular rectangular grid of data, and yield gradients on the entire grid, but only at constant altitude. We add to these the ordinary numerical integration (in horizontal coordinates) of the gradient integrals. In total we compare two prism, two FFT and two ordinary numerical integration methods using 1, elevation data in two topographic regimes (rough and moderate terrain). Prism methods depend on the type of finite elements that are generated with the elevation data; in particular, alternative triangulations can yield significant differences in the gradients (up to tens of Eötvös). The FFT methods depend on a series development of the topographic heights, requiring terms up to 14th order in rough terrain; and, one popular method has significant bias errors (e.g. 13 Eötvös in the vertical,vertical gradient) embedded in its practical realization. The straightforward numerical integrations, whether on a rectangular or triangulated grid, yield sub-Eötvös differences in the gradients when compared to the other methods (except near the edges of the integration area) and they are as efficient computationally as the finite element methods. [source] Extension of Vedernikov's Graph for Seepage from CanalsGROUND WATER, Issue 2 2001Bhagu R. Chahar In this investigation, using previously derived equations by Vedernikov and Morel-Seytoux, closed-form solutions have been obtained to compute the seepage from a slit and a strip. Also, a graphical solution as an extension of Vedernikov's graph has been presented for computing quantity of seepage from triangular, rectangular, and trapezoidal canals. The solution replaces approximately the cumbersome evaluation of improper integrals with unknown implicit transformation variables. [source] A simplified model of gas,liquid two-phase flow pattern transitionHEAT TRANSFER - ASIAN RESEARCH (FORMERLY HEAT TRANSFER-JAPANESE RESEARCH), Issue 7 2004Koji Ito Abstract An experiment of upward gas,liquid two-phase flow was conducted in an air,water isothermal system under atmospheric pressure. The differential pressure was measured at the fully developed section by using a variable reluctance type transducer to classify the flow patterns and their transitions. The flow behavior was observed with a high-speed video camera. The probability density function (PDF) of the differential pressure signal was employed to identify the flow pattern. A simplified one-dimensional flow model was proposed to clarify dominant factors affecting the formation and transitions of flow patterns. The model dealt with the gas-component advection based on the spatiotemporal void fraction behaviors by considering the gas compressibility, the wake, and the liquid phase redistribution mechanism. The simulation results of the model indicated four kinds of the void wave patterns (ripple-like, rectangular, distorted rectangular, and uniform wave patterns) depending on gas and liquid volumetric fluxes. These void wave patterns corresponded well to the experimentally observed flow patterns. The transitions among void wave patterns agree well with the Mishima,Ishii flow pattern map. The friction loss estimated by the present model coincides fairly well with Chisholm's empirical formula. © 2004 Wiley Periodicals, Inc. Heat Trans Asian Res, 33(7): 445,461, 2004; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/htj.20029 [source] Liquid-Crystal Patterning: Lithographic Alignment of Discotic Liquid Crystals: A New Time,Temperature Integrating Framework (Adv. Mater.ADVANCED MATERIALS, Issue 46 200946/2009) Liquid crystals are a successful example of how the control of self-assembly via chemical design leads to novel applications. Massimiliano Cavallini, Fabio Biscari, and co-workers report on p. 4688 that direct patterning of a continuous metal-free mesogenic phthalocyanine film (discotic LCs) is achieved by spatial control of column orientation using unconventional lithography. These patterned films work as time,temperature integrators at the columnar rectangular,hexagonal transition temperature. [source] Lithographic Alignment of Discotic Liquid Crystals: A New Time,Temperature Integrating FrameworkADVANCED MATERIALS, Issue 46 2009Massimiliano Cavallini Liquid crystals are a successful example of how the control of self-assembly via chemical design leads to novel applications. Direct patterning of a continuous metal-free mesogenic phthalocyanine film (discotick liquid crystals) is shown by the spatial control of columns orientation by unconventional lithography. These patterned films work as time,temperature integrators at a columnar rectangular,hexagonal transition temperature. [source] Phase transformation behaviour and bending properties of hybrid nickel,titanium rotary endodontic instrumentsINTERNATIONAL ENDODONTIC JOURNAL, Issue 4 2007Y. Hayashi Abstract Aim, To investigate the bending properties of hybrid rotary nickel,titanium endodontic instruments in relation to their transformation behaviour. Methodology, Four types of nickel,titanium rotary endodontic instruments with different cross-sectional shapes (triangular-based and rectangular-based) and different heat treatment conditions (super-elastic type and hybrid type with shape memory effect) were selected to investigate bending properties and phase transformation behaviour. Bending load of the instruments was measured in a cantilever-bending test at 37 °C with the maximum deflection of 3.0 mm. A commercial rotary instrument, ProFile (PF; Dentsply Maillefer, Ballaigues, Switzerland) was used as a reference for the bending test. Phase transformation temperatures were calculated from the diagrams obtained from differential scanning calorimetry. Data were analysed by anova and Scheffe's test. Results, The bending load values of the hybrid type that had undergone additional heat treatment at the tip were significantly lower (P < 0.05) than those of the super-elastic type with no additional heat treatment. The bending load values of rectangular-based cross-sectional shaped instruments were significantly lower (P < 0.05) than those of triangular-based cross-sectional shaped instruments. Phase transformation temperatures (Ms and Af points) of the hybrid type were significantly higher (P < 0.05) than the super-elastic type. The Mf and As points of the tip part were significantly higher (P < 0.05) than those of the whole part of the hybrid instrument. Conclusions, Additional heat treatment of hybrid nickel,titanium instruments may be effective in increasing the flexibility of nickel,titanium rotary instruments. [source] Analysis of laterally loaded piles with rectangular cross sections embedded in layered soilINTERNATIONAL JOURNAL FOR NUMERICAL AND ANALYTICAL METHODS IN GEOMECHANICS, Issue 7 2008D. Basu Abstract An analysis is developed to determine the response of laterally loaded rectangular piles in layered elastic media. The differential equations governing the displacements of the pile,soil system are derived using variational principles. Closed-form solutions of pile deflection, the slope of the deflected curve, the bending moment and the shear force profiles can be obtained by this method for the entire pile length. The input parameters needed for the analysis are the pile geometry and the elastic constants of the soil and pile. The new analysis allows insights into the lateral load response of square, rectangular and circular piles and how they compare. Copyright © 2007 John Wiley & Sons, Ltd. [source] Finite element modelling of thick plates on two-parameter elastic foundationINTERNATIONAL JOURNAL FOR NUMERICAL AND ANALYTICAL METHODS IN GEOMECHANICS, Issue 14 2001Ryszard Buczkowski Abstract This paper is intended to give some information about how to build a model necessary for bending analysis of rectangular and circular plates resting on a two-parameter elastic foundation, subjected to combined loading and permitting various types of boundary conditions. The formulation of the problem takes into account the shear deformation of the plate and the surrounding interaction effect outside the plate. The numerical model based on an 18-node zero-thickness isoparametric interface element interacting with a thick Reissner,Mindlin plate element with three degrees of freedom at each of the nine nodes, which enforce C0 continuity requirements for the displacements and rotations of the midsurface, is proposed. Stiffness matrices of a special interface element are superimposed on the global stiffness matrix to represent the stiffening elastic foundation under and beyond the plate. Some numerical examples are given to illustrate the advantages of the method presented. Copyright © 2001 John Wiley & Sons, Ltd. [source] Numerical analysis of the rectangular domain decomposition methodINTERNATIONAL JOURNAL FOR NUMERICAL METHODS IN BIOMEDICAL ENGINEERING, Issue 7 2009Younbae Jun Abstract When solving parabolic partial differential equations using finite difference non-overlapping domain decomposition methods, one often uses the stripwise decomposition of spatial domain and it can be extended to the rectangular decomposition without further analysis. In this paper, we analyze the rectangular decomposition when the modified implicit prediction (MIP) algorithm is used. We show that the performance of the rectangular decomposition and the stripwise decomposition is different. We compare spectral radius, maximum error, efficiency, and total operations of the rectangular and the stripwise decompositions. We investigate the accuracy of the interface of the rectangular decomposition and the effects of the correction phase of the rectangular decomposition. Numerical experiments have been done in both two and three spatial dimensions and show that the rectangular decomposition is not better than the stripwise decomposition. Copyright © 2008 John Wiley & Sons, Ltd. [source] Discrete singular convolution methodology for free vibration and stability analyses of arbitrary straight-sided quadrilateral platesINTERNATIONAL JOURNAL FOR NUMERICAL METHODS IN BIOMEDICAL ENGINEERING, Issue 11 2008Ömer Civalek Abstract A new discrete singular convolution (DSC) method is developed for vibration, buckling and static analyses of arbitrary straight-sided quadrilateral plates. The straight-sided quadrilateral domain is mapped into a square domain in the computational space using a four-node element. By using the geometric transformation, the governing equations and boundary conditions of the plate are transformed from the physical domain into a square computational domain. Numerical examples illustrating the accuracy and convergence of the DSC method for straight-sided quadrilateral thin plates such as rectangular, skew, trapezoidal and rhombic plates are presented. The results obtained by the DSC method were compared with those obtained by the other numerical and analytical methods. Copyright © 2007 John Wiley & Sons, Ltd. [source] An unconditionally convergent algorithm for the evaluation of the ultimate limit state of RC sections subject to axial force and biaxial bendingINTERNATIONAL JOURNAL FOR NUMERICAL METHODS IN ENGINEERING, Issue 8 2007G. Alfano Abstract We present a numerical procedure, based upon a tangent approach, for evaluating the ultimate limit state (ULS) of reinforced concrete (RC) sections subject to axial force and biaxial bending. The RC sections are assumed to be of arbitrary polygonal shape and degree of connection; furthermore, it is possible to keep fixed a given amount of the total load and to find the ULS associated only with the remaining part which can be increased by means of a load multiplier. The solution procedure adopts two nested iterative schemes which, in turn, update the current value of the tentative ultimate load and the associated strain parameters. In this second scheme an effective integration procedure is used for evaluating in closed form, as explicit functions of the position vectors of the vertices of the section, the domain integrals appearing in the definition of the tangent matrix and of the stress resultants. Under mild hypotheses, which are practically satisfied for all cases of engineering interest, the existence and uniqueness of the ULS load multiplier is ensured and the global convergence of the proposed solution algorithm to such value is proved. An extensive set of numerical tests, carried out for rectangular, L-shaped and multicell sections shows the effectiveness of the proposed solution procedure. Copyright © 2007 John Wiley & Sons, Ltd. [source] Voronoi cell finite difference method for the diffusion operator on arbitrary unstructured gridsINTERNATIONAL JOURNAL FOR NUMERICAL METHODS IN ENGINEERING, Issue 1 2003N. SukumarArticle first published online: 11 MAR 200 Abstract Voronoi cells and the notion of natural neighbours are used to develop a finite difference method for the diffusion operator on arbitrary unstructured grids. Natural neighbours are based on the Voronoi diagram, which partitions space into closest-point regions. The Sibson and the Laplace (non-Sibsonian) interpolants which are based on natural neighbours have shown promise within a Galerkin framework for the solution of partial differential equations. In this paper, we focus on the Laplace interpolant with a two-fold objective: first, to unify the previous developments related to the Laplace interpolant and to indicate its ties to some well-known numerical methods; and secondly to propose a Voronoi cell finite difference scheme for the diffusion operator on arbitrary unstructured grids. A conservation law in integral form is discretized on Voronoi cells to derive a finite difference scheme for the diffusion operator on irregular grids. The proposed scheme can also be viewed as a point collocation technique. A detailed study on consistency is conducted, and the satisfaction of the discrete maximum principle (stability) is established. Owing to symmetry of the Laplace weight, a symmetric positive-definite stiffness matrix is realized which permits the use of efficient linear solvers. On a regular (rectangular or hexagonal) grid, the difference scheme reduces to the classical finite difference method. Numerical examples for the Poisson equation with Dirichlet boundary conditions are presented to demonstrate the accuracy and convergence of the finite difference scheme. Copyright © 2003 John Wiley & Sons, Ltd. [source] A numerical integration scheme for special finite elements for the Helmholtz equationINTERNATIONAL JOURNAL FOR NUMERICAL METHODS IN ENGINEERING, Issue 4 2003Peter Bettess Abstract The theory for integrating the element matrices for rectangular, triangular and quadrilateral finite elements for the solution of the Helmholtz equation for very short waves is presented. A numerical integration scheme is developed. Samples of Maple and Fortran code for the evaluation of integration abscissć and weights are made available. The results are compared with those obtained using large numbers of Gauss,Legendre integration points for a range of testing wave problems. The results demonstrate that the method gives correct results, which gives confidence in the procedures, and show that large savings in computation time can be achieved. Copyright © 2002 John Wiley & Sons, Ltd. [source] A lumped mass numerical model for cellular materials deformed by impactINTERNATIONAL JOURNAL FOR NUMERICAL METHODS IN ENGINEERING, Issue 11 2001Z. H. Tu Abstract When impacted by a relatively rigid body, cellular materials undergo severe deformation and extensive material failure. However, such behaviour may not be well described using traditional numerical approaches such as the finite element method. This paper presents a lumped mass numerical model which can accommodate high degrees of deformation and material failure. The essence of this model is to discretize a block of material into contiguous element volumes, each represented by a mass point. Interactions between a node and its neighbours are accounted for by defining ,connections' that represent their interfaces which transmit stresses. Strains at a node are calculated from the co-ordinates of the surrounding nodes; these also determine the stresses on the interfaces. The governing equations for the entire solution domain are then converted into a system of equations of motion with nodal positions as unknowns. Failure criteria and possible combinations of ,connection' breakage are incorporated to model the occurrence of damage. A practical contact algorithm is also developed to describe the contact interactions between cellular materials and rigid bodies. Simulations for normal and oblique impacts of rigid rectangular, cylindrical and wedge-tipped impactors on crushable foam blocks are presented to substantiate the validity of the model. The generally good correlation between the numerical and experimental results demonstrates that the proposed numerical approach is able to model the impact response of the crushable foam. However, some limitations in modelling crack propagation in oblique impacts by a rigid impactor on foam blocks are observed. Copyright © 2001 John Wiley & Sons, Ltd. [source] Bifurcation and stability analysis of laminar flow in curved ductsINTERNATIONAL JOURNAL FOR NUMERICAL METHODS IN FLUIDS, Issue 4 2010Werner Machane Abstract The development of viscous flow in a curved duct under variation of the axial pressure gradient q is studied. We confine ourselves to two-dimensional solutions of the Dean problem. Bifurcation diagrams are calculated for rectangular and elliptic cross sections of the duct. We detect a new branch of asymmetric solutions for the case of a rectangular cross section. Furthermore we compute paths of quadratic turning points and symmetry breaking bifurcation points under variation of the aspect ratio , (,=0.8,1.5). The computed diagrams extend the results presented by other authors. We succeed in finding two origins of the Hopf bifurcation. Making use of the Cayley transformation, we determine the stability of stationary laminar solutions in the case of a quadratic cross section. All the calculations were performed on a parallel computer with 32×32 processors. Copyright © 2009 John Wiley & Sons, Ltd. [source] Using a piecewise linear bottom to fit the bed variation in a laterally averaged, z -co-ordinate hydrodynamic modelINTERNATIONAL JOURNAL FOR NUMERICAL METHODS IN FLUIDS, Issue 11 2004XinJian Chen Abstract In developing a 3D or laterally averaged 2D model for free-surface flows using the finite difference method, the water depth is generally discretized either with the z -co-ordinate (z -levels) or a transformed co-ordinate (e.g. the so-called , -co-ordinate or , -levels). In a z -level model, the water depth is discretized without any transformation, while in a , -level model, the water depth is discretized after a so-called , -transformation that converts the water column to a unit, so that the free surface will be 0 (or 1) and the bottom will be -1 (or 0) in the stretched co-ordinate system. Both discretization methods have their own advantages and drawbacks. It is generally not conclusive that one discretization method always works better than the other. The biggest problem for the z -level model normally stems from the fact that it cannot fit the topography properly, while a , -level model does not have this kind of a topography-fitting problem. To solve the topography-fitting problem in a laterally averaged, 2D model using z -levels, a piecewise linear bottom is proposed in this paper. Since the resulting computational cells are not necessarily rectangular looking at the x,z plane, flux-based finite difference equations are used in the model to solve the governing equations. In addition to the piecewise linear bottom, the model can also be run with full cells or partial cells (both full cell and partial cell options yield a staircase bottom that does not fit the real bottom topography). Two frictionless wave cases were chosen to evaluate the responses of the model to different treatments of the topography. One wave case is a boundary value problem, while the other is an initial value problem. To verify that the piecewise linear bottom does not cause increased diffusions for areas with steep bottom slopes, a barotropic case in a symmetric triangular basin was tested. The model was also applied to a real estuary using various topography treatments. The model results demonstrate that fitting the topography is important for the initial value problem. For the boundary value problem, topography-fitting may not be very critical if the vertical spacing is appropriate. Copyright © 2004 John Wiley & Sons, Ltd. [source] Three-dimensional transient free-surface flow of viscous fluids inside cavities of arbitrary shapeINTERNATIONAL JOURNAL FOR NUMERICAL METHODS IN FLUIDS, Issue 10 2003Kyu-Tae Kim Abstract The three-dimensional transient free-surface flow inside cavities of arbitrary shape is examined in this study. An adaptive (Lagrangian) boundary-element approach is proposed for the general three-dimensional simulation of confined free-surface flow of viscous incompressible fluids. The method is stable as it includes remeshing capabilities of the deforming free-surface, and thus can handle large deformations. A simple algorithm is developed for mesh refinement of the deforming free-surface mesh. Smooth transition between large and small elements is achieved without significant degradation of the aspect ratio of the elements in the mesh. The method is used to determine the flow field and free-surface evolution inside cubic, rectangular and cylindrical containers. These problems illustrate the transient nature of the flow during the mixing process. Surface tension effects are also explored. Copyright © 2003 John Wiley & Sons, Ltd. [source] Synthesis of Nanophased Metal Oxides in Supercritical Water: Catalysts for Biomass ConversionINTERNATIONAL JOURNAL OF APPLIED CERAMIC TECHNOLOGY, Issue 5 2006Caroline Levy Nanoparticles of zinc oxide-based materials (ZnO, ZnAl2O4) with various morphologies were synthesized in supercritical water (SCW) with a flow-type apparatus and in sub- and supercritical water with a batch reactor. In the flow-type apparatus, smaller particles were obtained. Depending on the precursors, the morphology of crystallites is rod, hexagonal, or rectangular shaped. ZnAl2O4 was synthesized with a high specific surface area (SBET) reaching 210 m2/g and nanocrystallite sizes ,10 nm. The KOH concentration played a major role in the formation of ZnO and ZnAl2O4 phases. Then, the synthesized materials were used as catalysts for the biomass conversion by the oxidation process to produce hydrogen. [source] Modeling of conductor losses in capacitors with rectangular and circular platesINTERNATIONAL JOURNAL OF RF AND MICROWAVE COMPUTER-AIDED ENGINEERING, Issue 2 2009A. Deleniv Abstract Analytic models are developed for the losses in the plates of MIM capacitors. The formulas are derived for the equivalent loss tangent and resistance of the arbitrary thick rectangular electrodes. An equivalent surface resistance is introduced for an arbitrary thick conductor. The accuracy of the model is demonstrated by comparison with rigorous Sonnet simulation and available alternative approach. The formula for the resistance of electrically thick circular electrodes is obtained. The derived expressions are verified via comparison with rigorous HFSS (high frequency structure simulator) simulations using eigenmode solver. © 2008 Wiley Periodicals, Inc. Int J RF and Microwave CAE, 2009. [source] Resolution of neutron three-axis spectrometers using acceptance diagramsJOURNAL OF APPLIED CRYSTALLOGRAPHY, Issue 5 2002L. D. Cussen Two-dimensional `acceptance diagrams' are used to discuss the transmission function and the resolution of neutron three-axis spectrometers. The discussion is simplified by assuming rectangular rather than the usual Gaussian transmission profiles for the beam elements, i.e. collimators and crystal mosaic spreads, but the results can be applied to the Gaussian profile approximation. The formalism clearly shows the effects of beam elements on the instrument transmission to the detector. Suitable choices of beam elements are determined to match the transmission functions of the primary and secondary spectrometers and hence optimize measurements. The effect of sample mosaic is addressed. The `focusing angle' for inelastic scattering is determined and discussed. [source] Revised capillary suction time (CST) test to reduce consumable costs and improve dewaterability interpretationJOURNAL OF CHEMICAL TECHNOLOGY & BIOTECHNOLOGY, Issue 3 2006Miklas Scholz Abstract The aim of this paper is to critically assess the standard capillary suction time (CST) test and to propose a modified device (prototype) and a revised CST procedure. The empirical CST test (using a circular funnel) is well established as the leading method for the determination of sludge dewaterability in spite of its current shortcomings such as restricted modelling possibilities, and therefore the ability to predict physical processes such as the amount of water bound by the paper. Nevertheless, the CST apparatus is portable, and the method is easy to conduct, quick, cost-effective and accurate, if the product of solid concentration and average specific resistance to filtration is of interest. A novel prototype with a rectangular instead of a circular funnel incorporating a stirrer (optional), and using a cheaper paper with similar or improved characteristics is proposed to reduce consumable costs and improve dewaterability interpretation. Copyright © 2005 Society of Chemical Industry [source] ,The first bite of the cherry' Intra-oral manipulation prior to the first bite in humansJOURNAL OF ORAL REHABILITATION, Issue 7 2001J. F. Prinz The breakdown of food in the mouth during mastication can be described in terms of two parameters: a breakage function, which describes the fragmentation of food after a bite, and a selection function which defines the probability of particle fracture. The non-zero value of the selection function depends on the manipulation of food particles by the tongue. Little, however, is known about this. As a first step, this study investigated the manipulation of wax sheets of differing sizes and shapes by the tongue after ingestion. It was found that subjects tended to orientate rectangular and square wax wafers so that the long axis of the particle was parallel to the tooth row, independent of the initial orientation given when they were introduced into the mouth. Circular wafers were randomly oriented relative to initial orientation. If this could be extrapolated to the start of mastication, then it suggests that the tongue tends to align food particles so that the post-canines produce close to the greatest surface area possible by fragmenting them along their longest axis. [source] Release liner removal method for transdermal drug delivery systems (TDDS)JOURNAL OF PHARMACEUTICAL SCIENCES, Issue 7 2010Anna M. Wokovich Abstract A release liner removal test is a valuable test for assessing the quality of a transdermal drug delivery system (i.e., TDDS, patch). This test measures the force required to remove the release liner from a patch. The objective of the present study was to establish sample preparation and instrument parameters for measuring release liner removal adhesion for TDDS. Ten TDDS were evaluated (six drugs for a total of 29 lots). Patches which had a rate-controlling membrane were run as-is, since they could not be cut to a precise width without sacrificing their structural integrity. Patches that were square or rectangular in shape were run as-is, and the width of these patches was determined using a digital caliper. Patches which were not square or rectangular in shape and did not have a rate-controlling membrane were cut to a precise width using a specimen cutter. Double-sided tape was used to adhere the liner side of the transdermal system to a clean stainless steel test panel. A release liner peel adhesion method for TDDS is proposed using a dwell time of approximately 3,min, a peel angle of 90°, and a peel speed of 300,mm/min. © 2010 Wiley-Liss, Inc. and the American Pharmacists Association J Pharm Sci 99:3177,3187, 2010 [source] Microwave Bandgap in Multilayer Ceramic StructuresJOURNAL OF THE AMERICAN CERAMIC SOCIETY, Issue 3 2006Bo Li A multilayer ceramic structure with a photonic bandgap (MC-PBG) was fabricated by a method of tape casting combined with screen printing. The MC-PBG structure is a two-dimensional array with either rectangular or hexagonal metal coils in a ceramic matrix. The metal coils are connected to the base metal layer in the ceramic substrate to form a monolithic body. The surface-wave dispersion properties of these MC-PBG structures were measured. A stop band, which is significantly influenced by the symmetrical characteristics of the inductor,capacitor (LC) arrays, was found in both the structures in the frequency range of 2.0,3.5 GHz. Because of their effective surface-wave suppression, MC-PBG structures can be used as high-performance antenna substrates to enhance the broadside gain of patch antenna devices. [source] Suppressing One-Bond Correlations in HMBC Spectra: Improved Performance for the BIRD,HMBC Pulse SequenceMAGNETIC RESONANCE IN CHEMISTRY, Issue 3 2009Julien Furrer Abstract An improved version of the BIRD,HMBC experiment is proposed. In comparison to the original version, the filtering (suppression of 1JCH signals) is accomplished using a double tuned G-BIRD filter positioned in the middle of the long-range correlations evolution period. Compensation of offset dependence by replacing the rectangular 180° pulses with the broadband inversion pulses (BIPs), with superior inversion performance and improved tolerance to B1 field inhomogeneity, significantly improves the sensitivity of the original BIRD,HMBC experiment. For usual one-bond coupling constants ranges (115,180 Hz), optimal results are easily obtained by adjusting the delays, ,, of the BIRD elements to an average J value. For larger ranges (e.g. 110,260 Hz), the use of a double tuned G-BIRD filter allows excellent suppression degrees for all types of one-bond constants present in a molecule, superior to the original scheme and other purging schemes. These attributes make the improved version of the BIRD,HMBC experiment a valuable and robust tool for rapid spectral analysis and rapid checks of molecular skeletons with a minimum spectrometer time. Copyright © 2009 John Wiley & Sons, Ltd. [source] Sound propagation in a channel with a discontinuity in the form of a semicircleMATHEMATICAL METHODS IN THE APPLIED SCIENCES, Issue 15 2003Volkmar Weise Abstract For the description of wave propagation in ducts with variable cross-sections it is necessary to determine reflection and transmission at the points of discontinuity in the cross-sectional contour. Analytic solutions are well known for rectangular and circular duct cross-sections with rotational symmetric arrangements. The aim of this paper is the description of sound propagation in cylindrical ducts with semicircular discontinuities and thus non-rotationally symmetric discontinuities of the cross-sectional contour. In particular, excitation with higher azimuthal and radial modes also will be included. This solution is achieved by using the orthogonality properties of the trigonometric and Bessel functions. Copyright © 2003 John Wiley & Sons, Ltd. [source] | |||||||||||||||||||||||||||||||||||||