Home About us Contact
|
Home About us Contact | ||
|
|
||
Processing Parameters (processing + parameter)
Kinds of Processing Parameters Selected AbstractsPredicting Spray Processing Parameters from Required Coating Structural Attributes by Artificial Intelligence,ADVANCED ENGINEERING MATERIALS, Issue 7 2006A.-F. Kanta Predicting processing parameters to manufacture a coating with the required structural attributes is of prime interest to reduce the associate development costs. Such an approach permits, among other advantages, to select the most appropriate scheme among several possible to implement. This paper intends to present such an approach. The specific case of predicting plasma spray process parameters to manufacture a grey alumina (Al2O3 -TiO2, 13% by wt.) coating was considered. [source] Hot Isostatic Pressing of Cubic Boron Nitride,Tungsten Carbide/Cobalt (cBN,WC/Co) Composites: Effect of cBN Particle Size and Some Processing Parameters on their Microstructure and PropertiesJOURNAL OF THE AMERICAN CERAMIC SOCIETY, Issue 2 2007V. Martínez Cubic boron nitride (cBN)-cemented carbide composites have gained attraction over the last few years because of their potential uses as wear parts. The densification behavior of cBN,hard metal composites by glass encapsulation hot isostatic pressing,has been investigated. Composites with different cBN grades (from 0/0.5 to 6/12 ,m particle sizes) and cBN content (up to 50 vol%) were selected for this study. Near-full densification was obtained at temperatures between 1100° and 1200°C, and pressures between 150 and 200 MPa, respectively, while no phase transformation of cBN into the low-hardness hexagonal form has been detected by X-ray diffraction. The addition of cBN to the hard metal base material led to an increase of hardness, a significant increase of fracture toughness (KIC measured by Vickers indentation), and a moderate decrease of mechanical strength (determined by three-point bending). [source] Dielectric properties of polyethylene terephthalate/polyphenylene sulfide/barium titanate nanocomposite for application in electronic industryPOLYMER ENGINEERING & SCIENCE, Issue 8 2010Monika Konieczna Polymer/ceramic nanocomposites designed for application as electronic packaging were prepared using corotating twin-screw extruder. The dielectric properties of the composites made from polyethylene terephthalate (PET), polyphenylene sulfide, and barium titanate were studied as a function of BaTiO3 fraction in the range between 0.75 and 1.5 wt%. Processing parameters were optimized in order to obtain the nanocomposites with appropriate dielectric properties like dielectric permittivity ,,, dielectric losses ,,, and their temperature stability in a wide frequency range. The measurements showed the increase of the dielectric permittivity value ,, in the composites in comparison to both pure polymers. The dielectric loss factor tg, of the composites was found to be much smaller than that of the pure PET. The weak influence of the ceramics on the temperature stability of the dielectric properties of the composites was stated. POLYM. ENG. SCI., 50:1613,1619, 2010. © 2010 Society of Plastics Engineers [source] Nanocomposite systems based on unsaturated polyester and organo-clayPOLYMER ENGINEERING & SCIENCE, Issue 2 2005I. Mironi-Harpaz Unsaturated polyester (UP) systems give rise to numerous possible approaches in synthesizing nanocomposites. A simultaneous mixing method was used to synthesize UP-resin/organo-clay nanocomposites. The effects of various mixing processes, using several organically-modified clay types, were investigated. The incorporation of these organo-clays resulted in an intercalated structure, the extent of which depended mainly on the type of the clay organic treatment. Organo-clays that exhibited the highest intercalation levels were further studied using a sequential mixing method. The UP-alkyd (without styrene) was mixed with different organo-clays. Processing parameters such as mixing modes, applied shearing levels, clay contents, and mixing-temperatures were investigated. Prolonged high shear levels promoted the intercalation and exfoliation of the silicate layers, resulting in a better dispersion of clay particles. The high shear levels effects were achieved by vigorous mechanical mixing and were intensified by using large amounts of clay and optimized matrix viscosity. Rheological studies of the nanocomposites were found complementary and in correlation with morphological and thermal characterization. This methodological approach provides a basis for understanding the structuring processes involving the formation of the UP/clay nanocomposites and establishing materials-processing-structure interrelations. Polym. Eng. Sci. 45:174,186, 2005. © 2005 Society of Plastics Engineers. [source] Consolidation of Particles by Severe Plastic Deformation: Mechanism and Applications in Processing Bulk Ultrafine and Nanostructured Alloys and Composites,ADVANCED ENGINEERING MATERIALS, Issue 8 2010Kenong Xia Severe plastic deformation (SPD) can be used to consolidate particles into bulk ultrafine and nanostructured materials. SPD consolidation relies on plastic deformation of individual particles, rather than diffusion, to achieve bonding and thus can be carried out at much lower temperatures. Using examples of consolidation of Al particles by back pressure equal channel angular pressing (BP-ECAP), it is demonstrated that full consolidation is achieved when the particles are sheared to disrupt the surface oxide layer whereas consolidation is impossible or incomplete in the case of particles sliding over each other. The effects of particle characteristics such as size, shape, strength and surface condition, as well as processing parameters including temperature and back pressure, are discussed to shed light on the mechanism of SPD consolidation. Potential applications of SPD in powder consolidation and processing of bulk ultrafine and nanostructured materials are discussed. [source] The Effects of Casting Temperature on the Glass Formation of Zr-Based Metallic Glasses,ADVANCED ENGINEERING MATERIALS, Issue 12 2009Jie Mao Abstract The glass1-forming ability of two alloys, Zr64.9Al7.9Ni10.7Cu16.5 and Zr47Cu37.5Ag7.5Al8, prepared by arc-melting a mixture of Zr, Cu, Al, Ni and Ag elements is studied as a function of casting temperature. Other processing parameters such as the alloy melt mass, and the vacuum and injection pressures during the copper-mold-casting process are kept constant so just the influence of the casting temperature is considered. The casting temperature determines the characteristics of the liquid melt and the cooling rate. The glass-forming ability is discussed in terms of dissipation of pre-exiting, metastable local-ordering clusters that act as nucleation sites promoting crystallization, the cooling rate at high casting temperatures, and the presence of oxygen in the alloys, which is increased at high casting temperatures. It is found that the glass-forming ranges of alloys shrink as the glass-forming size approaches a critical value. The optimum temperatures are around 1450,K and 1550,K for Zr64.9Al7.9Ni10.7Cu16.5 and Zr47Cu37.5Ag7.5Al8 alloys respectively. The alloys were studied by XRD, TEM, oxygen-level determination, and DSC. [source] Hot Workability, Microstructural Control and Rate-Controlling Mechanisms in Cast-Homogenized AZ31 Magnesium Alloy,ADVANCED ENGINEERING MATERIALS, Issue 3 2009Yellapregada Venkata Rama Krishna Prasad Optimum conditions for microstructural control in industrial hot working of cast and homogenized AZ31 magnesium alloys are evaluated by using a processing map. The recommended window for bulk metal working of this alloy is the domain in the temperature range 300,450,°C and strain rate range 1,10,s,1, and the optimum processing parameters are 400,°C and 10,s,1, where grain-boundary self diffusion is the rate-controlling mechanism. [source] Nitrided Amorphous Stainless Steel Coatings Deposited by Reactive Magnetron Sputtering from an Austenitic Stainless Steel TargetADVANCED ENGINEERING MATERIALS, Issue 1-2 2009Salvatore Cusenza Abstract Stainless steel films were reactively magnetron sputtered in argon/nitrogen gas flow onto oxidized silicon wafers using austenitic AISI 316 stainless-steel targets. The deposited films of about 300,nm thickness were characterized by conversion electron Mö-i;ssbauer spectroscopy, magneto-optical Kerr-effect, X-ray diffraction, Rutherford backscattering spectrometry, and resonant nuclear reaction analysis. These complementary methods were used for a detailed examination of the nitriding effects for the sputtered stainless-steel films. The formation of an amorphous and soft ferromagnetic phase in a wide range of the processing parameters was found. Further, the influence of postvacuum-annealing was examined by perturbed angular correlation to achieve a comprehensive understanding of the nitriding process and phase formation. The amorphous phase is not very stable and crystallization can be observed at 973,K. [source] Predicting Spray Processing Parameters from Required Coating Structural Attributes by Artificial Intelligence,ADVANCED ENGINEERING MATERIALS, Issue 7 2006A.-F. Kanta Predicting processing parameters to manufacture a coating with the required structural attributes is of prime interest to reduce the associate development costs. Such an approach permits, among other advantages, to select the most appropriate scheme among several possible to implement. This paper intends to present such an approach. The specific case of predicting plasma spray process parameters to manufacture a grey alumina (Al2O3 -TiO2, 13% by wt.) coating was considered. [source] Controlled Fabrication of Multitiered Three-Dimensional Nanostructures in Porous Alumina,ADVANCED FUNCTIONAL MATERIALS, Issue 14 2008Audrey Yoke Yee Ho Abstract We present the fabrication of multitiered branched porous anodic alumina (PAA) substrates consisting of an array of pores branching into smaller pores in succeeding tiers. The tiered three-dimensional structure is realized by sequentially stepping down the anodization potential while etching of the barrier layer is performed after each step. We establish the key processing parameters that define the tiered porous structure through systematically designed experiments. The characterization of the branched PAA structures reveals that, owing to constriction, the ratio of interpore distance to the anodization potential is smaller than that for pristine films. This ratio varies from 1.8 to 1.3,nm,V,1 depending on the size of the preceding pores and the succeeding tier anodization potential. Contact angle measurements show that the multitiered branched PAA structures exhibit a marked increased in hydrophilicity over two-dimensional PAA films. [source] Systematic optimization for the evaluation of the microinjection molding parameters of light guide plate with TOPSIS-based Taguchi methodADVANCES IN POLYMER TECHNOLOGY, Issue 1 2010Te-Li Su Abstract A back light module is a key product for providing sufficient light source for a liquid crystal display (LCD). The light guide plate (LGP), used to increase the light usage rate, is a key component in the back light module. This study researches the microinjection molding process parameters and the quality performance of the LGP. Its purpose was to develop a combining Technique for Order Preference by Similarity to Ideal Solution (TOPSIS) with the Taguchi method. This is to optimize the multiquality performance of the LGP for the injection molding manufacturing process, in which both the LCD and the LGP spontaneously produce the best quality performance for V-cut depth and angle. First, an L18 orthogonal array was planned for the manufacturing parameters that affect the microinjection molding process. These included cooling time, mold temperature, melt temperature, injection speed, injection pressure, packing pressure, packing switching, and packing time. The TOPSIS was used to deal with the single-quality optimization disadvantage of the Taguchi method. Then, the TOPSIS response table was used to obtain the optimized manufacturing parameters combination for a multiresponse process optimization. From the analysis of variance, the significant factors for the quality performance of the LGP could be obtained. In other words, by controlling these factors, it was possible to efficiently control the quality performance of the LGP. Finally, with the five verified experiments, the optimized processing parameters came within a 95% confidence interval. © 2010 Wiley Periodicals, Inc. Adv Polym Techn 29:54,63, 2010; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/adv.20181 [source] Adaptive geometry and process optimization for injection molding using the kriging surrogate model trained by numerical simulationADVANCES IN POLYMER TECHNOLOGY, Issue 1 2008Yuehua Gao Abstract An adaptive optimization method based on the kriging surrogate model has been developed to intelligently determine the optimal geometric dimensions and processing parameters for minimizing warpage in injection-molded components. The kriging surrogate model is a statistics-based interpolated technique that provides the approximate functional relationship between warpage and factors that influence warpage. In this study, it is used to be first trained by,and later replaced,the full-fledged, time-consuming numerical simulation in the optimization process. Based on this surrogate model, an adaptive iteration scheme that takes into account the predicted uncertainty is performed to improve the accuracy of the surrogate model while finding the optimum solution. The optimization process starts with a small number of initial training sample points and then adds additional key points during iterations by evaluating the correlations among the candidate points. As an example of validation and application, optimization of geometric dimensions and processing parameters for a box-shape part with different and stepwise wall thicknesses has been performed. The results demonstrate the feasibility and effectiveness of the proposed optimization method. © 2008 Wiley Periodicals, Inc. Adv Polym Techn 27:1,16, 2008; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/adv.20116 [source] Effect of processing parameters on the cellular morphology and mechanical properties of thermoplastic polyolefin (TPO) microcellular foamsADVANCES IN POLYMER TECHNOLOGY, Issue 4 2007Steven Wong Abstract In this study, the effects of processing parameters on the cellular morphologies and mechanical properties of thermoplastic polyolefin (TPO) microcellular foams are investigated. Microcellular closed cell TPO foams were prepared using a two-stage batch process method. The microstructure of these foamed samples was controlled by carefully altering the processing parameters such as saturation pressure, foaming temperature, and foaming time. Foam morphologies were characterized in terms of the cell density, foam density, and average cell size. Elastic modulus, tensile strength, and elongation at break of the foamed TPO samples were measured for different cell morphologies. The findings show that the mechanical properties are significantly affected by the foaming parameters that varied with the cell morphologies. The experimental results can be used to predict the microstructure and mechanical properties of microcellular polymeric TPO foams prepared with different processing parameters. © 2008 Wiley Periodicals, Inc. Adv Polym Techn 26:232,246, 2007; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/adv.20104 [source] Factors affecting the formation of fingering in water-assisted injection-molded thermoplasticsADVANCES IN POLYMER TECHNOLOGY, Issue 2 2006Shih-Jung Liu Abstract Water-assisted injection-molding technology has received extensive attention in recent years, due to the lightweight of plastic parts, relatively low-resin cost per part, faster cycle time, and flexibility in the design and manufacture. However, there are still some unsolved problems that confound the overall success of this technology. One of these is the water "fingering" phenomenon, in which the water bubbles penetrate outside designed water channels and form finger-shape branches. This study has investigated the effects of various processing parameters on the formation of fingering in water-assisted injection-molded thermoplastic parts. Both amorphous and semicrystalline polymers were used to mold the parts. The influence of water channel geometry, including aspect ratio and fillet geometry, on the fingering was also investigated. It was found that water-assisted injection-molded amorphous materials gave less fingering, while molded semicrystalline parts gave more fingering when compared to those molded by gas-assisted injection molding. For the water channels used in this study, the channels with a rib on the top produced parts with the least water fingering. Water fingering in molded parts decreases with the height-to-thickness ratio of the channels. The water pressure, water injection delay time and short-shot size were found to be the principal parameters affecting the formation of water fingering. In addition, a numerical simulation based on the transient heat conduction model was also carried out to help better explain the mechanism for the formation of fingering in water-assisted injection-molded thermoplastics. © 2006 Wiley Periodicals, Inc. Adv Polym Techn 25: 98,108, 2006; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/adv.20062 [source] Modification of polypropylene by melt vibration blending with ultra high molecular weight polyethyleneADVANCES IN POLYMER TECHNOLOGY, Issue 3 2002Kejian Wang Abstract A novel vibration internal mixer was used to prepare polypropylene/ultra high molecular weight polyethylene PP/UHMWPE blends with two additional adjustable processing parameters (vibration frequency and vibration amplitude) as compared with those prepared in the steady mode. Microscopy, mechanical tests, and differential scanning calorimetry showed that vibration influenced the blend morphology and the product properties. The good phase homogeneity of the blends might be due to the variation of shear rate either spatially or temporally in blending. Additionally, the vibration internal mixer could be used to analyze the dependency of viscosity on the shear rate. Vibration enhanced the interpenetration of UHMWPE into PP and vice versa. Subsequently, the formed crystals of two components were connected, and there was epitaxy between PP and UHMWPE crystals. Moreover, the crystalline aggregates, with the amorphous UHMWPE, formed a complex network-like continuous structure, which improved the elongation ratio at the break and the yield strength. The higher the vibration frequency and/or the larger the vibration amplitude at a fixed average rotation speed of the mixer, the more significant these effects were. The larger amount of the connected crystals, especially of , form of PP in the bulk , form PP as well as with the continuous phase structure, led to a higher tensile properties of PP/UHMWPE vibration blended. © 2002 Wiley Periodicals, Inc. Adv Polym Techn 21: 164,176, 2002; Published online in Wiley Interscience (www.interscience.wiley.com). DOI 10.1002/adv.10020 [source] Influence of processing conditions and part design on the gas-assisted injection molding processADVANCES IN POLYMER TECHNOLOGY, Issue 4 2001Nan-Shing Ong Gas-assisted injection molding has been developed to solve the problems that the conventional injection molding process is not able to. It is believed that the new process is able to produce final parts with higher quality at a more effective cost. Warpage and sink marks are reduced and there is material-savings to be reaped. This research aims to investigate some of the processing parameters that come with this new process. They include shot size, gas delay time, gas pressure, and melt temperature. The influence of part design is also looked into. Five designs were used in the research and compared. The responses evaluated include gas bubble length, residual wall thickness, bending strength, warpage, and fingering. © 2001 John Wiley & Sons, Inc. Adv Polym Techn 20: 270,280, 2001 [source] Online pressure,volume,temperature measurements of polypropylene using a testing mold to simulate the injection-molding processJOURNAL OF APPLIED POLYMER SCIENCE, Issue 1 2010Jian Wang Abstract To obtain accurate prediction of service performance and service life of polymers and to optimize the processing parameters, a modified online measurement was used to measure the pressure,volume,temperature (PVT) properties of polymers under certain processing conditions. The measurement was based on an injection molding machine, and it was used to obtain the PVT data of polymers directly with a special testing mold under normal processing conditions. The PVT properties of a semicrystalline polymer, polypropylene, were measured through both an online testing mold and a conventional piston,die dilatometer. The PVT properties were correlated by a modified two-domain Tait equation of state. The differences between the two groups of PVT data measured were investigated, and relative differences, especially in the rubbery state because of different cooling or heating measuring modes and sample forms, were observed. Numerical simulations of injection-molding processes were carried out by Moldflow software with both of the types of PVT data. The resulting online PVT data exhibited improvement in the accurate prediction of shrinkage and warpage. © 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2010 [source] Reactive mold filling in resin transfer molding processes with edge effectsJOURNAL OF APPLIED POLYMER SCIENCE, Issue 6 2009Yanyu Ding Abstract Reactive mold filling is one of the important stages in resin transfer molding processes, in which resin curing and edge effects are important characteristics. On the basis of previous work, volume-averaging momentum equations involving viscous and inertia terms were adopted to describe the resin flow in fiber preform, and modified governing equations derived from the Navier,Stokes equations are introduced to describe the resin flow in the edge channel. A dual-Arrhenius viscosity model is newly introduced to describe the chemorheological behavior of a modified bismaleimide resin. The influence of the curing reaction and processing parameters on the resin flow patterns was investigated. The results indicate that, under constant-flow velocity conditions, the curing reaction caused an obvious increase in the injection pressure and its influencing degree was greater with increasing resin temperature or preform permeability. Both a small change in the resin viscosity and the alteration of the injection flow velocity hardly affected the resin flow front. However, the variation of the preform permeability caused an obvious shape change in the resin flow front. The simulated results were in agreement with the experimental results. This study was helpful for optimizing the reactive mold-filling conditions. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009 [source] Increasing recyclability of PC, ABS and PMMA: Morphology and fracture behavior of binary and ternary blendsJOURNAL OF APPLIED POLYMER SCIENCE, Issue 5 2008Jan Rybnicek Abstract Binary and ternary blends of PC, ABS, and PMMA were studied. The blends were produced from original and recycled materials by melt mixing in a wide range of compositions. Instrumented Charpy impact testing, tensile testing, rheology investigations, and electron microscopy were carried out to determine the relationship between the deformation and fracture behavior, blend composition, morphology, and processing parameters. Resistance against unstable crack propagation was evaluated using the concepts of J -integral and crack-tip-opening displacement (CTOD). The transition from ductile elastic-plastic to brittle-linear elastic fracture behavior was observed in the case of PC/ABS/PMMA blend at 10% of PMMA. Reprocessing had only a slight influence on the deformation and fracture behavior of the recycled blends. The blends produced from recycled materials proved to be competitive with the original pure materials. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci 2008 [source] Effect of quasi-carbonization processing parameters on the mechanical properties of quasi-carbon/phenolic compositesJOURNAL OF APPLIED POLYMER SCIENCE, Issue 5 2008Donghwan Cho Abstract In this work, quasi-carbon fabrics were produced by quasi-carbonization processes conducted at and below 1200°C. Stabilized polyacrylonitrile (PAN) fabrics and quasi-carbon fabrics were used as reinforcements of phenolic composites with a 50 wt %/50 wt % ratio of the fabric to the phenolic resin. The effect of the quasi-carbonization process on the flexural properties, interfacial strength, and dynamic mechanical properties of quasi-carbon/phenolic composites was investigated in terms of the flexural strength and modulus, interlaminar shear strength, and storage modulus. The results were also compared with those of a stabilized PAN fabric/phenolic composite. The flexural, interlaminar, and dynamic mechanical results were quite consistent with one another. On the basis of all the results, the quasi-static and dynamic mechanical properties of quasi-carbon/phenolic composites increased with the applied external tension and heat-treatment temperature increasing and with the heating rate decreasing for the quasi-carbonization process. This study shows that control of the processing parameters strongly influences not only the mechanical properties of quasi-carbon/phenolic composites but also the interlaminar shear strength between the fibers and the matrix resin. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 [source] Influence of Bone Tissue Density and Elasticity on Ultrasound Propagation: An In Vitro StudyJOURNAL OF BONE AND MINERAL RESEARCH, Issue 12 2000Francesca de Terlizzi Abstract Ultrasound (US) waves are mechanical vibrations that are applied to a material,bone tissue,in order to study its properties, that is, density, elasticity, and structure. In this study we evaluated in which way density and elasticity of the spongy bone influenced the transmission of 1.25 MHz US pulses. Twelve cylindrical specimens (diameter, 8 mm; height, 5 mm) excised from phalanxes of pig were decalcified with 0.5 M EDTA for different times (0, 2, and 5 days). During these periods, the samples underwent the following investigations: US transmission, density, and elasticity measurements. To assess the homogeneity of decalcification, the cross-sections of some samples were microradiographed. A detailed analysis of the US signal received was performed using velocity, Fourier analysis, and some parameters typical of signal processing technique. A good correlation was found between US velocity and density (r2 = 0.70); a lower correlation was found between velocity and elasticity (r2 = 0.59). If density and elasticity are considered simultaneously, the correlation with the US velocity improves significantly (r2 = 0.84). Fourier analysis enabled us to observe a shift of the main frequency toward lower values as the decalcification process advanced. We also observed that in the regressions weighted for density, US velocity correlated poorly with elasticity (r2 = 0.16), whereas signal processing parameters maintain a good correlation with elasticity (ultrasound peak amplitude [UPA], r2 = 0.48; slope, r2 = 0.62). In this study, it has been observed that when using a signal processing technique to analyze US pulses, it is possible to identify some parameters that are related in different ways to density and to elastic properties of bone. Our results show the potentiality of US technique to separate information on bone density and elasticity that X-ray-based densitometric methods do not provide. [source] COMPUTATIONAL FLUID DYNAMICS MODELING OF FLUID FLOW IN HELICAL TUBESJOURNAL OF FOOD PROCESS ENGINEERING, Issue 2 2002T. KORAY PALAZOGLU ABSTRACT The effect of different processing parameters on the degree of mixing and axial and radial pressure drops, during single-phase flow in helical tubes was investigated by using CFD software. Correlations were developed to calculate axial and radial pressure drops, and also the ratio of maximum to average fluid velocities. All of these quantities were found to be dependent on curvature ratio (ratio of tube diameter to coil diameter). Flow visualization experiments were performed to assess the degree of mixing in different configurations. At identical conditions, the degree of mixing was higher in the system with the large curvature ratio, which is in agreement with the simulation results. A minimum ratio of maximum to average fluid velocities of 1.61 was achieved, representing a 20% reduction in hold tube length for Newtonian fluid in laminar flow. [source] IDENTIFICATION OF IMPORTANT PRODUCTION VARIABLES AFFECTING HARD PRETZEL QUALITYJOURNAL OF FOOD QUALITY, Issue 3 2005N. YAO ABSTRACT The objective of this study was to determine the importance of raw material and processing variables that influence pretzel quality by utilizing a screening experiment design. Eleven variables were selected based on preliminary experiments, and a two-level-11-factor (211) fractional factorial experimental design was used to screen the variables. Several responses were measured for dough before and after extrusion, for half-baked and fully baked pretzels. These responses are important indicators of consistency and quality during pretzel processing. Results indicated that flour protein content, the amount of water added to make dough and dough mixing time were important variables influencing dough behavior. Caustic concentration affected brightness of half-baked pretzels but did not influence the color of the final product. Baking time was the most important factor for both half-baked product and final product qualities. The hardness of fully baked pretzels was influenced by baking time, temperature in baking oven zone 1, drying time and drying temperature. The color of final products was significantly influenced by baking time, while both baking time and drying temperature affected the moisture content of the final product. A key observation was that none of the raw material or dough processing parameters, within the range tested, influenced final pretzel quality as defined by pretzel moisture content, hardness or color. [source] A STATISTICAL ANALYSIS OF CREAMING VARIABLES IMPACTING PROCESS CHEESE MELT QUALITYJOURNAL OF FOOD QUALITY, Issue 4 2003T.A. GLENN III To simulate commercial processing, a pilot scale 10-gallon (0.04m3), dual ribbon blender was equipped with a thermal control system and a 0.75 hp (559.27 W) electrical motor. An experimental design consisted of three temperatures (75, 80, 85C), three mixing rates (50, 100,150 RPM), and six durations (1, 5, 10, 15, 25, 35 min). Quantified process variables included: process strain and thermal history, and total, instantaneous, and change in mechanical energy. The Schreiber melt test was used to examine the relationship between the processing parameters and melt performance. A statistical analysis revealed significant parameter estimates (P < 0.0001) for each quantified variable in a general linear model. The process cheese industry will gain insight into controlled manufacturing conditions to deliver desired melt functionality. [source] Chemical Characteristics of Low-Fat Soymilk Prepared by Low-Speed Centrifugal Fractionation of the Raw SoymilkJOURNAL OF FOOD SCIENCE, Issue 5 2010Zhi-Sheng Liu Abstract:, Large oil,protein particles (2 to 60 ,m) were found in raw soymilk (or water extract of soybean), which was prepared in specific conditions. The large particles could be separated by sedimentation by centrifuging raw soymilk for 5 to 30 min at a low gravitational force ranging from 96 to 2410 ×,g. Chemical analysis showed that 80% to 90% of the total lipids and 30% to 40% of the total proteins were located in the precipitated fraction. The supernatant fraction had a dramatically higher protein-to-lipid ratio than the whole soymilk. The ratio of 11S/7S proteins and the ratio of 11S acidic/basic subunits were significantly (P,< 0.05) higher in the precipitate than that either in the whole soymilk or in the supernatant. Besides centrifuging conditions, other factors, including soymilk concentration, grinding method, soybean variety, and soybean storage, also significantly (P,< 0.05) affected the centrifugal fractionation. This study showed that low-speed centrifugation facilitated the separation of oil-protein particles from raw soymilk, and can be used as an innovative method for preparing low-fat soymilk and 11S protein-enriched ingredients. The findings also increased our understanding of the association or aggregation between proteins and lipids in raw soymilk after grinding. Practical Application:, Soymilk has become a popular beverage in the Western world due to its health benefits. Consumer demands for low-fat and organic foods have been increasing in the recent years. Currently, there are no alternative methods for manufacturing low-fat soymilk from whole soybeans. We found that most, if not all, of lipids in the raw soymilk were located in large particles, which could be separated by low-speed centrifugation. This centrifugal fractionation was investigated by varying processing parameters, soybean varieties, and soybean storage conditions. The approach has potential to be used for manufacturing low-fat soymilk. This study also has increased our understanding of the interactions between lipid and protein in raw soymilk. [source] Effects of Process Parameters on Quality Changes of Shrimp During Drying in a Jet-Spouted Bed DryerJOURNAL OF FOOD SCIENCE, Issue 9 2007C. Niamnuy ABSTRACT:, The objective of the present study was to investigate the effects of various parameters, that is, concentration of salt solution (2%, 3%, 4%[w/v]), boiling time (3, 5, 7 min), drying air temperature (80, 100, 120 °C), and size of shrimp, on the kinetics of drying and various quality attributes of shrimp, namely, shrinkage, rehydration ability, texture, colors, and microstructure, during drying in a jet-spouted bed dryer. In addition, the effects of these processing parameters on the sensory attributes of dried shrimp were also investigated. Small shrimp (350 to 360 shrimp/kg) and large shrimp (150 to 160 shrimp/kg) were boiled and then dried until their moisture content was around 25% (d.b.). It was found that the degree of color changes, toughness, and shrinkage of shrimp increased while the rehydration ability decreased with an increase in the concentration of salt solution and boiling time. Size of shrimp and drying temperature significantly affected all quality attributes of dried shrimp. The conditions that gave the highest hedonic scores of sensory evaluation for small dried shrimp are the concentration of salt solution of 2% (w/v), boiling time of 7 min, and drying air temperature of 120 °C. On the other hand, the conditions that gave the highest hedonic scores of sensory evaluation for large dried shrimp are the concentration of salt solution of 4% (w/v), boiling time of 7 min, and drying air temperature of 100 °C. The quality attributes of dried shrimp measured by instruments correlated well with the sensory attributes, especially the color of dried shrimp. [source] Incorporation of proteins within alginate fibre-based scaffolds using a post-fabrication entrapment methodJOURNAL OF PHARMACY AND PHARMACOLOGY: AN INTERNATI ONAL JOURNAL OF PHARMACEUTICAL SCIENCE, Issue 7 2006Qingpu Hou In this study, a physical entrapment process was explored for the incorporation of proteins within preformed fibrous alginates and the release profile was tuned by varying the processing parameters. The entrapment process was carried out in a series of aqueous solutions at room temperature and involved pre-swelling of the fibrous alginate within a Na+ -rich solution, followed by exposure to the protein of choice and entrapping it by re-establishing cross-links of alginate with BaCl2. Entrapment and release of fluorescein isothiocyanate-labelled bovine serum albumin (FITC-BSA), a model protein, was studied. It was found that a sustained release of the incorporated protein in cell culture medium for about 6 days was achieved. The main factors determining the release profile included the NaCl/CaCl2 ratio in the pre-swelling solution, protein concentration, and the exposure time. To retard protein release, alginate fibres with entrapped FITC-BSA were processed together with poly(d, l -lactide) (PDLLA) into porous alginate fibre/PDLLA composites using supercritical CO2. In this manner, release of the protein for up to 3 months was achieved. [source] THE IMPACT OF HOMOGENIZATION AND MICROFILTRATION ON RENNET-INDUCED GEL FORMATIONJOURNAL OF TEXTURE STUDIES, Issue 4 2008STEPHAN THOMANN ABSTRACT The effects of the independent variables, milk homogenization pressure (p1), concentration factor of milk microfiltration (i) and pH on the rheological properties of rennet milk gels were studied. Nondestructive oscillatory rheometry was used to determine rennet coagulation time (RCT), curd firming rate (CFR) and cutting time (CT). A central composite design, comprising two levels of i (1 and 2), pH (6.4 and 6.6) and p1 (0 and 8 MPa), was applied. Second-order polynomial models successfully described (R2 > 0.92) the relationship between processing parameters and rheological properties of the gels. pH had the most important influence on RCT, while CFR and CT were strongly influenced by i, pH and the interaction of i and pH. In contradiction to studies on active filler interactions for acid milk gels, a discrepancy was observed between results obtained by compression test and rheometry. Rennet gel firmness strongly decreased with a rise in p1 when measured using the compression test, whereby CFR increased with an increase in p1 when measured using rheometry. The latter result corresponds to higher storage modulus values after a certain time indicating higher gel stiffness. This effect was stronger for concentrated milk than for unconcentrated milk. PRACTICAL APPLICATIONS The use of microfiltration (MF) and homogenization may reduce raw material and processing time in conventional cheese manufacture. However, MF markedly influences milk composition, and homogenization alters the particle size distribution of fat globules. Hence, both technologies may influence rennet-induced gel formation, syneresis, cheese composition and quality. Curd firmness of homogenized milk is often too weak to resist the extensive curd treatment applied in semi-hard cheese manufacture which causes loss of curd fines during the syneresis process and finally decreases cheese yield. MF leads to high curd firmness if cutting is not performed at the appropriate time, which unnecessarily extends processing time. The study of the effect of the individual treatments, as well as of the combination of both on rennet-induced gel formation, is the first important step to evaluate their impact on further processing steps in cheese making. The combination of both technologies may overcome the antagonistic effect of the individual technology as low curd firmness due to homogenization can be compensated by MF that increases curd firmness and vice versa. [source] Formation and Densification Behavior of MgAl2O4 Spinel: The Influence of Processing ParametersJOURNAL OF THE AMERICAN CERAMIC SOCIETY, Issue 6 2008Ibram Ganesh Different types of dense stoichiometric and nonstoichiometric magnesium aluminate (MgAl2O4) spinel (MAS) ceramics were prepared following a conventional double-stage firing process using different commercially available alumina and magnesia raw materials. Stoichiometric, magnesia-rich, and alumina-rich spinels were sintered at 1500°,1800°C for 1,2.5 h. The influence of the different processing parameters (average particle size, degree of spinel phase, green density, mass of the powder compact, sintering temperature, holding time at the peak temperature, and starting composition) on the densification behavior of MAS was assessed by measuring the bulk density, apparent porosity, and water absorption capacity, and microstructural observations. Most of the MAS compositions tested exhibited excellent sintering properties. [source] Microstructural Control of a 70% Silicon Nitride, 30% Barium Aluminum Silicate Self-Reinforced CompositeJOURNAL OF THE AMERICAN CERAMIC SOCIETY, Issue 1 2001Feng Yu The processing response of a 70% silicon nitride,30% barium aluminum silicate (70%-Si3N4,30%-BAS) ceramic-matrix composite was studied using pressureless sintering, at temperatures ranging from 1740°C, which is below the melting point of BAS, to 1950°C. The relationship between the processing parameters and the microstructural constituents, such as morphology of the ,-Si3N4 whisker and crystallization of the BAS matrix, was evaluated. The mechanical response of this array of microstructures was characterized for flexural strength, as well as fracture behavior, at test temperatures up to 1300°C. The indentation method was used to estimate the fracture resistance, and R -curves were obtained from modified compact-tension samples of selected microstructures at room temperature. [source] | ||||||||||||||||||||||||||||