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Laboratory Air (laboratory + air)
Selected AbstractsVery high-cycle fatigue behaviour of shot-peened high-carbon,chromium bearing steelFATIGUE & FRACTURE OF ENGINEERING MATERIALS AND STRUCTURES, Issue 8-9 2002K. SHIOZAWA ABSTRACT Effect of shot-peening on fatigue behaviour in the gigacycle regime was investigated in order to clarify the duplex S,N curve characteristics. Cantilever-type rotary bending fatigue tests were performed in laboratory air at room temperature by using hourglass-shaped specimens of high-carbon,chromium bearing steel, JIS SUJ2. Fatigue crack initiation site changed from the surface of untreated specimen to the subsurface of the specimen because of hardening and compressive residual stress with shot-peening in the region of high-stress amplitude. On the other hand, no difference in fatigue life controlled by the subsurface crack initiation between untreated specimen and shot-peening one was observed in high-cycle region. It was suggested that the S,N curve corresponding to the internal fracture mode is inherent in the material, as compared with the S,N curve of surface fracture mode, which is affected by surface conditions, environmental conditions and so on. Subsurface crack initiation and propagation behaviour were discussed under the detailed measurement of crack initiation area and shape of the fish-eye fracture surface. [source] The effect of pitting corrosion on fatigue lifeFATIGUE & FRACTURE OF ENGINEERING MATERIALS AND STRUCTURES, Issue 7 2000Dolley Fatigue testing of pre-pitted 2024-T3 aluminium alloy specimens is performed in laboratory air at 22 °C and 40% RH to characterize the effect of pitting corrosion on fatigue life. Specimens, pre-corroded in a 0.5 M NaCl solution from 48 to 384 h, have fatigue lives that are reduced by more than one order of magnitude after 384 h pre-corrosion as compared to those of uncorroded specimens. The reduction in fatigue life is interpreted in terms of the influence of the time of exposure to the corrosive environment or pit size. The crack-nucleating pit sizes, ranging from 20 to 70 ,m, are determined from post-fracture examinations by scanning electron microscopy. Fatigue lives are estimated using a fracture mechanics approach and are shown to be in good agreement with the actual data. A probabilistic analysis shows that the distribution of fatigue life is strongly correlated to the distribution in nucleating pit size. [source] Corrosion fatigue behaviour of a 15Cr-6Ni precipitation-hardening stainless steel in different tempersFATIGUE & FRACTURE OF ENGINEERING MATERIALS AND STRUCTURES, Issue 6 2000C.-K. Lin Systematic fatigue experiments, including both high-cycle axial fatigue (S,N curves) and fatigue crack growth (FCG, da/dN,,K curves), were performed on a precipitation-hardening martensitic stainless steel in laboratory air and 3.5 wt% NaCl solution. Specimens were prepared in three tempers, i.e. solution-annealed (SA), peak-aged (H900) and overaged (H1150) conditions, to characterize the effects of ageing treatment on the corrosion fatigue (CF) resistance. S,N results indicated that fatigue resistance in all three tempers was dramatically reduced by the aqueous sodium chloride environment. In addition, the smooth-surface specimens in H900 temper exhibited longer CF lives than the H1150 ones, while those in SA condition stood in between. However, for precracked specimens, the H1150 temper provided superior corrosive FCG resistance than the other two tempers. Comparison of the S,N and FCG curves indicated that early growth of crack-like defects and short cracks played the major role in determining the CF life for smooth surface. The differences in the CF strengths for the S,N specimens of the given three tempers were primarily due to their inherent differences in resistance to small crack growth, as they were in the air environment. [source] A new single grating spectrograph for ultraviolet Raman scattering studiesJOURNAL OF RAMAN SPECTROSCOPY, Issue 5 2006Lutz Hecht Abstract A state-of-the-art single grating spectrograph for Raman scattering studies within the deep ultraviolet (DUV) region of the electromagnetic spectrum is discussed. It is based on a high throughput DUV version of a single-stage monochromator originally designed for use in the visible spectral region. Its key components are two identical, newly designed calcium fluoride camera lenses each consisting of five different individual optical elements. The first of these lenses collimates the Raman scattered DUV radiation entering the spectrometer through its entrance slit. The second lens focuses the collimated beam of dispersed Raman scattered DUV radiation emerging from a high-resolution reflection grating onto a charge coupled device (CCD) detector with enhanced DUV sensitivity. A novel high transmission edge filter is used as a blocking device for a sufficient rejection of the Rayleigh line generating a relatively sharp transmittance cutoff at a Stokes Raman wavenumber shift of about ,450 cm,1 employing 257 nm DUV excitation. Overall, this new spectrograph enables rapid collection of Stokes DUV Raman scattered photons at f/2 wide apertures with sufficiently large signal-to-noise ratios (SNRs) in relatively short acquisition times and with an effective spectral resolution of approximately ,6 cm,1. Backscattered Raman spectra of the following chemicals are presented as typical results illustrating the excellent performance characteristics of this new DUV spectrograph for a variety of experimental conditions within different scattering scenarios and for a relatively wide range of commonly used sample preparation techniques: neat cyclohexane, laboratory air, polycrystalline D -glucose, single crystal L -alanine and a dilute aqueous solution of 2,-deoxyadenosine. Copyright © 2005 John Wiley & Sons, Ltd. [source] Tribological characterisation of hard coatings with and without DLC top layer in fretting testsLUBRICATION SCIENCE, Issue 1 2006D. KlaffkeArticle first published online: 14 DEC 200 Abstract The potential of coatings to protect components against wear and to reduce friction has led to a large variety of protective coatings. In order to check the success of coating modifications and to find solutions for different purposes, initial tests with laboratory tribometers are usually done to give information about the performance of a coating. Different Ti-based coatings (TiN, Ti(C,N), and TiAlN) and NiP were tested in comparison to coatings with an additional diamond-like carbon (DLC) top coating. Tests were done in laboratory air at room temperature with oscillating sliding (gross slip fretting) with a ball-on-disc arrangement against a ceramic ball (Al2O3). Special attention was paid to possible effects of moisture (relative humidity). The coefficient of friction was measured on line, and the volumetric wear at the disc was determined after the test from microscopic measurements of the wear scar and additional profiles. The friction and wear behaviour is quite different for the different coatings and depends more or less on the relative humidity. The DLC coating on top of the other coatings reduces friction and wear considerably. In normal and in moist air the coefficient of wear of the DLC top-layer coating is significantly less than 10,6,mm3/Nm and the coefficient of friction is below 0.1. In dry air, however, there is a certain tendency to high wear and high friction. Copyright © 2006 John Wiley & Sons, Ltd. [source] Investigation on the oxidation behaviour of gamma titanium aluminides coated with thermal barrier coatingsMATERIALS AND CORROSION/WERKSTOFFE UND KORROSION, Issue 7 2008R. Braun Abstract In the present study, the applicability of thermal barrier coatings (TBCs) on ,-TiAl alloys was investigated. Two alloys with the chemical compositions of Ti-45Al-8Nb-0.2B-0.15C and Ti-45Al-1Cr-6Nb-0.4W-0.2B-0.5C-0.2Si were used. Before TBC deposition, the specimens were pre-oxidised in laboratory air or low partial pressure oxygen atmosphere. Yttria partially stabilised zirconia top coats were then deposited using electron-beam physical vapour deposition (EB-PVD). The oxidation behaviour of the ,-TiAl specimens with TBC was studied by cyclic oxidation testing in air at 850 and 900,°C. Post-oxidation analysis of the coating systems was performed using scanning electron microscopy with energy-dispersive X-ray spectroscopy (EDS). No spallation of the TBC was observed for pre-oxidised specimens of both alloys when exposed to air at 850,°C for 1100 cycles of 1,h dwell time at high temperature. SEM micrographs of the thermally grown oxide scale revealed outer mixed TiO2/Al2O3 protrusions with a columnar structure. The protrusions contained small particles of zirconia and a low amount of about 0.5 at% zirconium was measured by EDS analysis throughout this outer oxide mixture. The TBCs exhibited excellent adherence on the oxide scale. Intercolumnar gaps and pores in the root area of the TBC were filled with titania and alumina. Below the outer columnar oxide scale, a broad porous zone of predominant titania was observed. The transition region between the oxide scale and substrate consisted of a discontinuous nitride layer intermixed with alumina particles and intermetallic phases rich in niobium formed at the nitride layer/substrate interface. When thermally cycled at 900,°C, the oxide scales on the alloy Ti-45Al-8Nb-0.2B-0.15C pre-oxidised in low partial pressure oxygen spalled off after 540 cycles. For the sample with TBC, spallation was observed after 810 cycles. Failure occurred in the thermally grown oxide near the oxide/nitride layer interface. Microstructural examinations revealed again oxide scales with columnar structure beneath the zirconia top coat and good adherence of the TBC on the thermally grown oxides formed at 900,°C. [source] | ||||||||||