Interlaminar Shear Strength (interlaminar + shear_strength)

Distribution by Scientific Domains


Selected Abstracts


Effect of grafting alkoxysilane on the surface properties of Kevlar fiber

POLYMER COMPOSITES, Issue 3 2007
Tao Ai
This research applied the methodology of metalation and grafting alkoxysilane to modify the surface of Kevlar-29 fiber. The surface properties of the modified Kevlar fiber were characterized by scanning electron microscopy, X-ray photoelectron spectroscopy, Fourier transform infrared spectroscopy, atomic force microscopy, and Brunauer-Emmett-Teller isothermal adsorption analysis. The relationship between surface characteristics of Kevlar fiber and its interfacial adhesion of Kevlar fiber-reinforced epoxy resin composites was also discussed. Compared with the untreated fiber, the surface of the modified Kevlar fiber was much rougher, its oxygen content increased by about 12%, the surface area enlarged about 10 times, and the wetting behavior improved. Due to the modification of the fiber, the adhesion between the fiber and the resin matrix was markedly improved and the Interlaminar Shear Strength of its epoxy composites increased by about 57%. POLYM. COMPOS. 28:412,416, 2007. © 2007 Society of Plastics Engineers. [source]


Processing and Properties of a Porous Oxide Matrix Composite Reinforced with Continuous Oxide Fibers

JOURNAL OF THE AMERICAN CERAMIC SOCIETY, Issue 10 2003
Magnus G. Holmquist
A process to manufacture porous oxide matrix/polycrystalline oxide fiber composites was developed and evaluated. The method uses infiltration of fiber cloths with an aqueous slurry of mullite/alumina powders to make prepregs. By careful manipulation of the interparticle pair potential in the slurry, a consolidated slurry with a high particle density is produced with a sufficiently low viscosity to allow efficient infiltration of the fiber tows. Vibration-assisted infiltration of stacked, cloth prepregs in combination with a simple vacuum bag technique produced composites with homogeneous microstructures. The method has the additional advantage of allowing complex shapes to be made. Subsequent infiltration of the powder mixture with an alumina precursor was made to strengthen the matrix. The porous matrix, without fibers, possessed good thermal stability and showed linear shrinkage of 0.9% on heat treatment at 1200°C. Mechanical properties were evaluated in flexural testing in a manner that precluded interlaminar shear failure before failure via the tensile stresses. It was shown that the composite produced by this method was comparable to porous oxide matrix composites manufactured by other processes using the same fibers (N610 and N720). The ratio of notch strength to unnotch strength for a crack to width ratio of 0.5 was 0.7,0.9, indicating moderate notch sensitivity. Interlaminar shear strength, which is dominated by matrix strength, changed from 7 to 12 MPa for matrix porosity ranging from 38% to 43%, respectively. The porous microstructure did not change after aging at 1200°C for 100 h. Heat treatment at 1300°C for 100 h reduced the strength for the N610 and N720 composites by 35% and 20%, respectively, and increased their brittle nature. [source]


Influence of high temperature and pressure ammonia solution treatment on interfacial behavior of carbon fiber/epoxy resin composites

JOURNAL OF APPLIED POLYMER SCIENCE, Issue 6 2009
L. H. Meng
Abstract The method of high temperature and pressure ammonia solution treatment to improve the interfacial performances of carbon fiber/epoxy composites is discussed in this study. Besides, the influence of high temperature and pressure ammonia solution treatment on carbon fiber and its reinforced epoxy composite interface performance were studied. The untreated and treated carbon fibers were characterized by monofilament tensile test, X-ray photoelectron spectroscopy (XPS), and atomic force microscope (AFM). The interfacial adhesion of the untreated and treated carbon fibers reinforced epoxy resin composites were also evaluated by interface shear strength (IFSS) test, interlaminar shear strength (ILSS) test, and fracture morphology analysis. It was found that the interfacial adhesion of composites increased greatly after high temperature and pressure ammonia solution treatment. The improvement of interfacial adhesion was attributed to the increase of polar functional groups and surface roughness of carbon fibers surface after treatment. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009 [source]


Effect of quasi-carbonization processing parameters on the mechanical properties of quasi-carbon/phenolic composites

JOURNAL OF APPLIED POLYMER SCIENCE, Issue 5 2008
Donghwan Cho
Abstract In this work, quasi-carbon fabrics were produced by quasi-carbonization processes conducted at and below 1200°C. Stabilized polyacrylonitrile (PAN) fabrics and quasi-carbon fabrics were used as reinforcements of phenolic composites with a 50 wt %/50 wt % ratio of the fabric to the phenolic resin. The effect of the quasi-carbonization process on the flexural properties, interfacial strength, and dynamic mechanical properties of quasi-carbon/phenolic composites was investigated in terms of the flexural strength and modulus, interlaminar shear strength, and storage modulus. The results were also compared with those of a stabilized PAN fabric/phenolic composite. The flexural, interlaminar, and dynamic mechanical results were quite consistent with one another. On the basis of all the results, the quasi-static and dynamic mechanical properties of quasi-carbon/phenolic composites increased with the applied external tension and heat-treatment temperature increasing and with the heating rate decreasing for the quasi-carbonization process. This study shows that control of the processing parameters strongly influences not only the mechanical properties of quasi-carbon/phenolic composites but also the interlaminar shear strength between the fibers and the matrix resin. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 [source]


Comparison of mechanical properties of epoxy composites reinforced with stitched glass and carbon fabrics: Characterization of mechanical anisotropy in composites and investigation on the interaction between fiber and epoxy matrix

POLYMER COMPOSITES, Issue 8 2008
Volkan Çeçen
The primary purpose of the study is to evaluate and compare the mechanical properties of epoxy-based composites having different fiber reinforcements. Glass and carbon fiber composite laminates were manufactured by vacuum infusion of epoxy resin into two commonly used noncrimp stitched fabric (NCF) types: unidirectional and biaxial fabrics. The effects of geometric variables on composite structural integrity and strength were illustrated. Hence, tensile and three-point bending flexural tests were conducted up to failure on specimens strengthened with different layouts of fibrous plies in NCF. In this article, an important practical problem in fibrous composites, interlaminar shear strength as measured in short beam shear test, is discussed. The fabric composites were tested in three directions: at 0°, 45°, and 90°. In addition to the extensive efforts in elucidating the variation in the mechanical properties of noncrimp glass and carbon fabric reinforced laminates, the work presented here focuses, also, on the type of interactions that are established between fiber and epoxy matrix. The experiments, in conjunction with scanning electron photomicrographs of fractured surfaces of composites, were interpreted in an attempt to explain the failure mechanisms in the composite laminates broken in tension. POLYM. COMPOS., 2008. © 2008 Society of Plastics Engineers [source]


The effects of curing cycles on properties of the epoxy system 3221/RH glass fabric composites

POLYMER COMPOSITES, Issue 4 2008
Hong Xuhui
In this work, the epoxy system 3221 and its glass fabric laminates were thermally cured under different curing temperatures. The curing degree of the resin was increased with elevated reaction temperature. Dynamic mechanical analysis was performed on the laminate coupons and glass transition temperature (Tg) and relative stiffness (E,) of composites were measured before and after soaked in distilled water at 70°C. A shift in glass transition temperature to higher values and the splitting of the tan , curve were observed with extent of cure under dry conditions. Tg values shifted to lower temperatures after immersion. Under wet condition, the change in Tg1 was very small when the curing degree was up to 96%. The relative stiffness experienced a reduction both in initial modulus and the initial sharp drop temperature after immersion. It also suggested that the excessively high curing temperature (>130°C) had a negative effect on the retention of relative stiffness under wet condition. Both the interlaminar shear strength and dielectric properties of laminates were determined before and after immersion. The compared results demonstrated that the elevated curing temperature played a good influence on both of the properties before aged. However, for samples cured above 130°C, lower retention of interlaminar shear strength and poor dielectric properties were observed during immersion due to their higher moisture contents. POLYM. COMPOS., 2008. © 2008 Society of Plastics Engineers [source]


Influence of epoxy sizing of carbon-fiber on the properties of carbon fiber/cyanate ester composites

POLYMER COMPOSITES, Issue 5 2006
Penggang Ren
The high modulus carbon fiber (M40J) sized by epoxy resin E51 and E20 reinforced bisphenol A dicyanate (2,2,-bis(4-cyanatophenyl) isopropylidene resin composite was prepared in order to investigate the influence of epoxy sizing of the fiber on the properties of the composite. Differential scanning calorimetry (DSC) and fourier transforms infrared (FTIR) analysis showed that epoxy resin have catalytic effect on cure reaction of cyanate ester. Mechanical properties of the composite revealed that M40J fiber sized by epoxy resin could improve the flexural strength and interlaminar shear strength of M40J/bisphenol A dicyanate composites. The micro-morphology of the composite fractures was studied by means of scanning electron microscopy (SEM). Reduced flaws were observed in the M40J-bisphenol A dicyanate interface when the sized fiber was used. Water absorption of the composites was also investigated. It was found that the water absorption descended at the initial boiling stage (12 h). POLYM. COMPOS, 27: 591,598, 2006. © 2006 Society of Plastics Engineers [source]