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Instron Universal Testing Machine (instron + universal_testing_machine)
Selected AbstractsPhysicochemical properties of low-fat and full-fat Cheddar cheesesINTERNATIONAL JOURNAL OF DAIRY TECHNOLOGY, Issue 3 2006E KÜÇÜKÖNER Low-fat (6% fat) and full-fat (32% fat) Cheddar cheese was manufactured and aged up to 6,9 months at 5°C. The objective was to study the impact of fat on the physicochemical properties of Cheddar cheese. Total soluble nitrogen (TSN) and protein nitrogen (TPSN) in aqueous extracts were determined by the Kjeldahl method. The peptide content of each cheese was determined with reverse phase chromatography (RPC). Low-fat Cheddar (LFC) had a markedly higher peptide content than full-fat Cheddar (FFC). The overall peptide quantity increased with age with a marked increase in hydrophobic peptide content. Rheological properties were determined using an Instron Universal Testing Machine. LFC had significantly higher stress values, indicating hard and rubbery texture, than FFC. Furthermore, LFC had lower strain values, indicating crumbliness. [source] The effect of coagulants on the texture of chhana (an acid and heat coagulated product made from milk)INTERNATIONAL JOURNAL OF FOOD SCIENCE & TECHNOLOGY, Issue 8 2005Mahuya Bandyopadhyay Summary Chhana (a heat and acid coagulated milk protein mass and an Indian equivalent to cottage cheese) can be used as a raw material for the manufacture of various types of sweets popular all over India. Texture Profile Analysis (TPA), using an Instron Universal Testing Machine, was used to determine the effect of different coagulants on the textural characteristics of chhana. Chhana was made using three different coagulants: citric acid, lactic acid and calcium lactate, at five different concentrations, 0.5, 1, 2, 4 and 8%. Two types of dilution media, distilled water and acid whey, were used. The textural characteristics obtained when aqueous 0.5% citric acid, aqueous 0.5% lactic acid and 4,8% calcium lactate solutions, using acid whey as the solvent, gave similar TPA readings to normal chhana. [source] The effect of thermocycling on peel strength of six soft lining materialsJOURNAL OF ORAL REHABILITATION, Issue 6 2002A. Sertgöz The bond strength of two heat-cured and four cold-cured soft lining materials was compared using a peeling test method before and after thermocycling. Tested soft lining materials were Molloplast B, Mollosil, Ufigel P, Ufigel C, Permaquick and Permaflex. Six specimens, 6·5 × 2 × 0·3 cm, for each group were prepared according to the manufacturers' instructions. Control groups were stored in a humidor for 24 h, whereas the others were thermocycled in a water bath between the 5 and 55 °C for 5000 cycles. Peel strength of samples were measured using an Instron Universal testing machine at a cross-head speed of 5 mm min,1. The types of failure were observed using an electron microscope. The highest peel bond strength values were calculated for Permaflex and Permaquick before and after thermocycling, respectively. Molloplast B, Mollosil, Ufigel P and Permaquick demonstrated an increase in peel strength after thermocycling, with Permaquick lining material having statistically significant increase. However, decrease in peel strength was observed for Ufigel C and Permaflex after thermocycling. Failure mode within the control groups was cohesive for Molloplast B, Permaquick and Permaflex, whereas adhesive for Ufigel P and Ufigel C. Mollosil demonstrated a mixed mode of failure for both thermocycled and control groups. [source] Tensile bond strengths of four different dentin adhesives on irradiated and non-irradiated human dentin in vitroJOURNAL OF ORAL REHABILITATION, Issue 9 2001C. R. Gernhardt This study evaluated the influence of irradiation on dentin bond strength. Sixty irradiated and 60 non-irradiated human third molars were used. The irradiation dose of 60 Gy was fractionally applied over 6 weeks (2 Gy day,1, 5 days week,1). All teeth were prepared in a special manner allowing the simulation of intra-pulpal pressure and dentin perfusion. Dentin specimens with a thickness of 2·0 mm were obtained under standardized conditions. The specimens were randomly assigned to four experimental groups. Tensile bond strength of four different dentin bonding agents (ScotchbondÔ 1, Solobond Plus®, Prime&BondÔ 2·1 and Syntac®) was evaluated using an Instron Universal testing machine. Pairwise comparison did not show any significant differences between the irradiated and non-irradiated groups. The influence of the different dentin adhesives was significant (P=0·0001; ANOVA). Compared with Solobond Plus® and Prime&BondÔ 2·1, the use of ScotchbondÔ 1 resulted in a significantly higher tensile bond strength in non-irradiated specimen (P< 0·05; closed test procedure based on Kruskal,Wallis test). Within the limitations of an in vitro study, it can be concluded that adhesive restoration procedures can be successfully used in patients irradiated for cancer of the head and neck. [source] Effect of preparation convergence on retention and seating discrepancy of complete veneer crownsJOURNAL OF ORAL REHABILITATION, Issue 10 2004D. C. N. Chan summary, The purpose of this study was to evaluate the retention and marginal seating discrepancy of complete veneer crown cemented with zinc phosphate using various preparation convergence designs. The method employed was that of cementing cast metal crowns onto 46 metal dies fabricated as complete veneer crown preparations with various convergence angles ranging from 0° to 70° and a shoulder finish line. The marginal discrepancy was calculated by measuring the change in crown height before and after cementation using an optical measuring microscope. The force required to remove the crowns from the dies in a vertical direction was determined using an Instron universal testing machine and recorded as retention. The increase in preparation convergence exhibited a wide variation of seating discrepancy between specimens, ranging from 4·58 ± 1·13 to 73·13 ± 78·32 ,m. Significant tilting of crown was observed as the convergence angle of preparation increased. The retention values ranged from 4·03 ± 0·61 to 12·12 ± 0·33 MPa. The Pearson analysis revealed statistically significant correlations between preparation convergence and marginal discrepancy (r = +0·62), and retention (r = ,0·91). Complete veneer crown retention and marginal discrepancy were influenced by the preparation convergence design. [source] Flexural Strength, Elastic Modulus, and pH Profile of Self-etch Resin Luting CementsJOURNAL OF PROSTHODONTICS, Issue 4 2008Egle Saskalauskaite DDS Abstract Purpose: To determine the flexural strength, modulus of elasticity, and 24-hour pH profile of three self-etching resin luting cements and to obtain comparative data for representative conventional resin and resin-modified glass ionomer luting cements. Materials and Methods: Three self-etching resin luting cements [RelyX Unicem (3M ESPE), Maxcem (Kerr), Embrace Wetbond (Pulpdent)] were tested and compared with two conventional resin cements [RelyX ARC (3M ESPE), Linkmax (GC)] plus two resin-modified glass ionomer luting cements [Fuji Plus (GC), RelyX Luting Plus (3M ESPE)]. Flexural strength and modulus of elasticity were determined using bar-shaped specimens (2 × 2 × 25 mm3) at 24 hours, using an Instron universal testing machine. Setting pH was measured using a flat-surface pH electrode at 0, 2, 5, 15, and 30 minutes and 1, 2, 4, 6, and 24 hours after mixing. Testing was performed under both dual-cured and self-cured conditions for all dual-cure cements. Data analysis included ANOVA and Tukey's test (p < 0.05). Results: The self-etching cements showed similar flexural strength to the conventional resin cements, except for Embrace Wetbond self-cured, which was considerably lower. Modulus of elasticity results were both higher and lower than for conventional resin cements. All photopolymerized conventional and self-etch dual-cure cements showed markedly higher flexural strength and modulus than when solely self-cured. The resin-modified glass ionomer cements were characterized by lower flexural strength and elastic modulus. Self-etching resin cements showed lower initial pH (2.0 to 2.4) than conventional resin cements (4.8 to 5.2) and a wide range of final pH values (3.9 to 7.3) at 24 hours. One self-etching cement (Unicem) revealed a unique pH profile characterized by a more rapid rise in pH to neutrality both when dual-cured (15 minutes) and when auto-cured (1 hour). Conclusions: The self-etching resin cements evaluated in this study displayed disparate properties and cannot be considered a homogeneous group. Flexural strength properties were most uniform and were similar to those of the conventional resin cements, whereas moduli of elasticity showed greater variation. Setting pH profiles differed, depending on the brand and mode of cure, even within the same category of luting cement. All cements with dual-cure capability, both conventional and self-etch, showed significantly superior properties when photopolymerized. [source] Cement Selection for Cement-Retained Crown Technique with Dental ImplantsJOURNAL OF PROSTHODONTICS, Issue 2 2008James L. Sheets DDS Abstract Purpose: The purpose of this study was to assess and compare the retentive nature of common dental cements that have been adapted for use in the implant abutment cement-retained crown (CRC) technique with those specifically formulated for this purpose. Materials and Methods: Ten regular diameter implant analogs were embedded in stainless steel disks. Unmodified CRC abutments were attached and torqued to 30 Ncm. Test crowns were waxed and cast with base metal alloy. Castings were fitted, cleaned with aluminum oxide, and steam cleaned prior to application of the cement. The cements used were: (1) Temp Bond, (2) UltraTemp, regular, (3) UltraTemp firm, (4) ImProv with petroleum jelly coating of crown, (5) ImProv without petroleum jelly, (6) Premier Implant with KY Jelly coating of abutment, (7) Premier Implant without KY jelly, (8) TR-2, (9) Fleck's, (10) Ketac Cem Aplicap, and (11) Fuji Plus Capsule. After cementation, assemblies were stored for 24 hours. Each sample was subjected to a pull-out test using an Instron universal testing machine at a crosshead speed of 5.0 mm/min. Loads required to remove the crowns were recorded, and mean values for each group determined. A one-way ANOVA and a post hoc least square difference (LSD) test were done for pairwise comparison at a confidence interval of 95%. Results: The mean values (±SD) of loads at failure (n = 10) for various cements were as follows (N): Ultratemp, regular 358.6 (±38.2) (Group A), ImProv without petroleum jelly 172.4 (±59.6) (Group B), Fleck's 171.8 (±62.2) (Group B), Ketac Cem 167.8 (±69.1) (Group B), UltraTemp firm 158.8 (±62.7) (Group BC), Fuji Plus 147.5 (±69.7) (Group BC), Premier without KY jelly 131.6 (±31.8) (Group BC), ImProv using petroleum jelly 130.8 (±42.5) (Group BC), Temp Bond 117.8 (±48.3) (Group C), TR-2 41.2 (±16.6) (Group D), and Premier with KY jelly 31.6 (±24.8) (Group D). Groups with the same letter were not significantly different. Conclusions: Within the limitations of this in vitro study, it is not suggested that any one cement is better than another at retaining cement-retained crowns (CRCs) to implant abutments or that a threshold value must be accomplished to ensure retention. The ranking of cements presented is meant to be a discretionary guide for the clinician in deciding the amount of desired retention between castings and implant abutments. [source] | |||||||||||||