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Hot Water Extraction (hot + water_extraction)
Selected AbstractsSUBCRITICAL WATER EXTRACTION OF CAFFEINE FROM BLACK TEA LEAF OF IRANJOURNAL OF FOOD PROCESS ENGINEERING, Issue 3 2008ANVAR SHALMASHI ABSTRACT This study examines subcritical water extraction (SCWE) of caffeine from black tea leaf. The effects of various operating conditions such as water temperature (100, 125, 150 and 175C), water flow rate (1, 2 and 4 g/min), mean particle size (0.5, 1 and 2 mm) on extraction yield and rate were determined. SCWE at 175C, water flow rate of 2 g/min and mean particle size of 0.5 mm were found to be able to recover 3.82% (w/w) of caffeine present in the black tea leaf within 3 h of extraction. In comparison to the SCWE, conventional hot water extraction showed 3.30% (w/w) extraction yield. It was found also that pressure had no effect on extraction yield and rate. PRACTICAL APPLICATIONS Recently, subcritical water has become of great interest as an alternative solvent for extraction of natural active compounds. Subcritical water, as a green solvent, can be used in many different fields of applications. In recent years, extraction of flavors, fragrances and antioxidant components from plant materials, and hydrolysis of carbohydrates, vegetable oils and fatty acids have been widely investigated by many researchers. Using subcritical water for analytical purposes, for soil remediation and applying it as a reaction media are some other interesting fields for practical applications. Subcritical water is an excellent solvent for caffeine as well as many other organic compounds but is safer than the organic solvents that are used for caffeine extraction. [source] Optimization of hot water extraction of roselle juice using response surface methodology: a comparative study with other extraction methodsJOURNAL OF THE SCIENCE OF FOOD AND AGRICULTURE, Issue 12 2003Peng-Kong Wong Abstract Roselle has regained the attention of many fruit juice manufacturers in Malaysia as a product that contains high ascorbic acid and anthocyanins. However, ascorbic acid and anthocyanin pigments can be easily destroyed during processing of fruit juice. Therefore, in the present study, the effects of different processing methods, namely hot water extraction (HWE), hot water blending, cold water blending and screw press, on the changes in anthocyanins and ascorbic acid contents of roselle juice were evaluated. The anthocyanins and ascorbic acid contents of roselle were determined using the pH differential method and high-performance liquid chromatography respectively. The physico-chemical characteristics and sensory properties of roselle juice were also evaluated. The results of the study indicate that the HWE method is the most effective extraction method, resulting in high anthocyanins and ascorbic acid contents of 43 g l,1 (as delphinidin-3-glucoside) and 2.34 g kg,1 respectively. The optimum juice extraction conditions were 3.5 h at 60 °C. Copyright © 2003 Society of Chemical Industry [source] Preparative separation of the saponin lancemaside a from Codonopsis lanceolata by centrifugal partition chromatographyPHYTOCHEMICAL ANALYSIS, Issue 5 2008Osamu Shirota Abstract Introduction. Lancemaside A is a saponin that inhibits decreases in blood testosterone level and thus prevents or ameliorates symptoms associated with male climacteric disorder. Our initial attempt to preparative isolation of lancemaside A from the saponin fraction of Codonopsis lanceolata roots by a preparative HPLC did not give a clear result. Objective. To develop a simple and efficient method for the preparative isolation of lancemaside A from the hot water extract of C. lanceolata roots using centrifugal partition chromatography (CPC). Methodology. The saponin fraction obtained from the hot water extract of C. lanceolata roots was used as the sample for preparative-scale separation of lancemasides by CPC using n -hexane:n -butanol:methanol:0.1% aqueous formic acid (3:4:1:6, v/v) as the two-phase solvent system. The upper phase (organic phase) of the two-phase solvent system was used as the mobile phase, and 0.5 g of saponin fraction was applied for separation by CPC. Each fraction that was separated by CPC was analysed by HPLC, and the fractions containing each of the separated compounds were pooled together, and then were purified by simple preparative HPLC. Results. The demonstrated separation sequence, hot water extraction, DIAION HP-20 column chromatography, CPC and preparative HPLC, yielded lancemaside A, foetidissimoside A and astersaponin Hb in their pure forms. Conclusion. The simple and efficient method for the preparative isolation of lancemaside A along with two other saponins, foetidissimoside A and astersaponin Hb, from the saponin fraction of C. lanceolata was established using CPC. [source] | ||||||||||