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Heat Treatment Conditions (heat + treatment_condition)
Selected AbstractsPhase transformation behaviour and bending properties of hybrid nickel,titanium rotary endodontic instrumentsINTERNATIONAL ENDODONTIC JOURNAL, Issue 4 2007Y. Hayashi Abstract Aim, To investigate the bending properties of hybrid rotary nickel,titanium endodontic instruments in relation to their transformation behaviour. Methodology, Four types of nickel,titanium rotary endodontic instruments with different cross-sectional shapes (triangular-based and rectangular-based) and different heat treatment conditions (super-elastic type and hybrid type with shape memory effect) were selected to investigate bending properties and phase transformation behaviour. Bending load of the instruments was measured in a cantilever-bending test at 37 °C with the maximum deflection of 3.0 mm. A commercial rotary instrument, ProFile (PF; Dentsply Maillefer, Ballaigues, Switzerland) was used as a reference for the bending test. Phase transformation temperatures were calculated from the diagrams obtained from differential scanning calorimetry. Data were analysed by anova and Scheffe's test. Results, The bending load values of the hybrid type that had undergone additional heat treatment at the tip were significantly lower (P < 0.05) than those of the super-elastic type with no additional heat treatment. The bending load values of rectangular-based cross-sectional shaped instruments were significantly lower (P < 0.05) than those of triangular-based cross-sectional shaped instruments. Phase transformation temperatures (Ms and Af points) of the hybrid type were significantly higher (P < 0.05) than the super-elastic type. The Mf and As points of the tip part were significantly higher (P < 0.05) than those of the whole part of the hybrid instrument. Conclusions, Additional heat treatment of hybrid nickel,titanium instruments may be effective in increasing the flexibility of nickel,titanium rotary instruments. [source] In situ high temperature microscopy study of the surface oxidation and phase transformations in titanium alloysJOURNAL OF MICROSCOPY, Issue 3 2002S. Malinov Summary Two popular commercial titanium alloys, Ti-6Al-4V and Ti-6Al-2Sn-4Zr-2Mo-0.08Si, were used for in situ high temperature microscopy study. The experiments were performed on an optical microscope equipped with high temperature stage using both normal and florescence lights. Two kinds of experiments were performed, at continuous heating/cooling with different rates and in isothermal conditions at different temperatures. The changes taking place on the sample surface during the experiments were monitored. The morphology of the ,,,,, phase transformation was recorded at different heat treatment conditions using the effect of thermal etching. An effect of sample surface oxidation and deoxidation was observed during continuous heating. The appearance and disappearance of ordered titanium oxides Ti3O and Ti2O are discussed based on the phase equilibrium diagram. The kinetics of the surface oxidation was monitored in both isothermal and continuous cooling conditions. [source] Low-wavenumber Raman scattering spectroscopy in studies of new gallium-doped silica glass-based transparent vitroceramic mediumJOURNAL OF RAMAN SPECTROSCOPY, Issue 8 2001R. Ceccato Optically transparent, silica glass-based vitroceramic material doped with gallium oxide was obtained by standard glass fusion and appropriate thermal treatments. Low-wavenumber Raman scattering spectroscopy allowed the determination of the microstructure and in particular the size distribution of nanoparticles embedded in the amorphous matrix. The nanocrystal growth was accurately controlled by heat treatment conditions. Transmission electron microscopy and X-ray diffraction measurements revealed the presence of a single crystalline phase, spherical-shaped nanoaggregates, homogeneously distributed in the transparent composite medium. Copyright © 2001 John Wiley & Sons, Ltd. [source] Effect of thermal exposure on the microstructure, tensile properties and the corrosion behaviour of 6061 aluminium alloy sheetMATERIALS AND CORROSION/WERKSTOFFE UND KORROSION, Issue 3 2005R. Braun Abstract Sheet material of the Al-Mg-Si alloy 6061 in the tempers T4 and T6 was thermally exposed at temperatures ranging from 85 to 120°C for 1000 h. The microstructure, tensile properties and the corrosion behaviour in the different heat treatment conditions were investigated using differential scanning calorimetry and transmission electron microscopy as well as performing tensile tests and various corrosion tests. The additional heat treatments, which should simulate aging during long-term service usage, caused an increase in strength of 6061-T4 sheet, associated with changes in the naturally aged microstructure. Thermal exposure at 120°C for 1000 h resulted in tensile and corrosion properties being similar to those obtained for peak-aged sheet. Alloy 6061 in the T6 temper exhibited microstructural stability when additionally heat treated at 85 and 120°C for 1000 h. No significant alterations in the microstructure, tensile properties, and corrosion performance were observed after exposure to slightly elevated temperatures. [source] | ||||||||||